3,4,5-三甲氧基苯甲酰氯合成路线 （共 203 条）
参考文献
Sharp
Journal of the Chemical Society, 1936 , p. 1234
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Frank; Fanta; Tarbell
Journal of the American Chemical Society, 1948 , vol. 70, p. 2314,2317
反应条件
1: palladium-barium sulfate; xylene / Hydrogenation 2: pyridine; piperidine 3: sodium-amalgam; aqueous ethanol View Scheme
参考文献
Slotta; Heller
Chemische Berichte, 1930 , vol. 63, p. 3029,3043
反应条件
1: palladium-barium sulfate; xylene / Hydrogenation 2: pyridine; piperidine View Scheme
参考文献
Chemische Berichte, , vol. 63, p. 3029,3043
反应条件
1: NaN3 / tetrahydrofuran; H2O / 0 °C 2: toluene / Heating 3: aq. NaOH View Scheme
参考文献
Vereshchagin, A. L.; Bryanskii, O. V.; Semenov, A. A.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , p. 40 - 42
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , vol. 19, # 1 p. 46 - 48
反应条件
sodium ethanolate T=0 - 5°C;
参考文献
Zhu, Youquan; Zou, Xiaomao; Hu, Fangzhong; Yao, Changsheng; Liu, Bin; Yang, Huazheng
Journal of Agricultural and Food Chemistry, 2005 , vol. 53, # 24 p. 9566 - 9570
反应条件
1: sodium ethanolate / ethanol / 20 °C 2: ammonium hydroxide / 20 °C View Scheme
参考文献
Li, Yao-Wu; Liu, Jia; Liu, Na; Shi, Duo; Zhou, Xiao-Tian; Lv, Jia-Guo; Zhu, Ju; Zheng, Can-Hui; Zhou, You-Jun
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 11 p. 3579 - 3584
反应条件
diethyl ether Behandeln des nach der Hydrolyse (mit Hilfe von wss. Salzsaeure) erhaltenen Reaktionsprodukts mit wss. Ammoniak unter Zusatz von Ammoniumchlorid;
参考文献
Hayashi
Acta Phytochimica, 1934 , vol. 8, p. 65,81
反应条件
1: 1.) ZnCl2 / 1.) Et2O, reflux, 3 h, 2.) benzene, r.t., overnight 2: 98percent hydrazine hydrate / ethanol / 5 h / Heating 3: KOH / 1 h / 180 °C 4: 82 percent / K / tetrahydrofuran / 24 h / Ambient temperature View Scheme
参考文献
Azzena, Ugo; Denurra, Teresa; Melloni, Giovanni; Rassu, Gloria
Journal of the Chemical Society, Chemical Communications, 1987 , p. 1549 - 1550
参考文献
Kuehne; Lambert
Journal of the American Chemical Society, 1959 , vol. 81, p. 4278,4283
Organic Syntheses, 1973 , vol. Coll. Vol. V, p. 400
反应条件
zinc(II) chloride in benzene 12 h; Ambient temperature;
参考文献
Azzena, Ugo; Denurra, Teresa; Melloni, Giovanni; Rassu, Gloria
Journal of the Chemical Society, Chemical Communications, 1987 , p. 1549 - 1550
