1,4-双(三甲硅基)-1,3-丁二炔合成路线 (共 93 条)
反应条件
bis-triphenylphosphine-palladium(II) chloride in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=80°C; 1 h;
参考文献
Journal of Organometallic Chemistry, , vol. 690, # 12 p. 2956 - 2966
反应条件
N-butylamine; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) in benzene 14 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 26, # 6 p. 709 - 712
反应条件
silver(I) acetate; triethylamine; palladium dichloride in methanol 0.333333 h; Ultrasonic-irradiation;
参考文献
Singh, Fateh V.; Amaral, Monica F.Z.J.; Stefani, Helio A.
Tetrahedron Letters, 2009 , vol. 50, # 22 p. 2636 - 2639
反应条件
triethylamine; palladium complex immobilised on silica gel in various solvent(s) T=70°C; Sonogashira coupling; 12 h;
参考文献
Tetrahedron, , vol. 61, # 41 p. 9860 - 9868
反应条件
copper(l) iodide; triethylamine; bis-triphenylphosphine-palladium(II) chloride in acetonitrile T=20°C; Sonogashira reaction; 1 h;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 15, # 4 p. 1586 - 1605
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; n-butyllithium in tetrahydrofuran T=-78 - 20°C; 15 h;
参考文献
Journal of Materials Chemistry C, , vol. 1, # 42 p. 7064 - 7072
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; n-butyllithium in tetrahydrofuran T=-78 - 20°C; 15 h;
参考文献
Journal of Materials Chemistry C, , vol. 1, # 42 p. 7064 - 7072
反应条件
trans-1,2-dichloroethylene; N-butylamine; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) in benzene 14 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 26, # 6 p. 709 - 712
反应条件
N-ethyl-N,N-diisopropylamine; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) in 1,2-dichloro-ethane T=80°C; 5 h;
参考文献
Livingston, Robert; Cox, Liam R.; Odermatt, Severin; Diederich, Franois
Helvetica Chimica Acta, 2002 , vol. 85, # 10 p. 3052 - 3077
反应条件
bis(benzonitrile)palladium(II) dichloride; meta-dibromobenzene; copper diacetate; diisopropylamine; triphenylphosphine 3 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 53, # 11 p. 2489 - 2496