4-甲基-2-[(甲硫基)甲基]苯酚合成路线 (共 3 条)
反应条件
thionyl chloride; triethylamine
1.) dichloromethane, -60 - -50 deg C, 1 h, 2.) -50 - -40 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Sato, Kikumasa; Inoue, Seiichi; Ozawa, Kimio; Tazaki, Michiko
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , p. 2715 - 2719
参考文献
Yamamoto,T. et al.
Tetrahedron, 1978 , vol. 34, p. 3097 - 3103
反应条件
(i) (CF3CO)2O, CH2Cl2, (ii) /BRN= 1305151/, 2,6-dimethyl-pyridine, (iii) Et3N; Multistep reaction;
参考文献
Hiraki,Y. et al.
Bulletin of the Chemical Society of Japan, 1977 , vol. 50, p. 447 - 452