反应条件
1: BOC-glycine With EDC monohydrochloride; 1-hydroxybenzotriazol-hydrate in dichloromethane
T=20°C; 0.166667 h; Inert atmosphere;
2: 4-Chloro-benzene-1,2-diamine in dichloromethane; N,N-dimethyl-formamide
T=23°C; Inert atmosphere;
3: With acetic acid in dichloromethane; N,N-dimethyl-formamide
T=70°C; 2 h; Inert atmosphere;
参考文献
Bibian, Mathieu; Rahaim, Ronald J.; Choi, Jun Yong; Noguchi, Yoshihiko; Schuerer, Stephan; Chen, Weimin; Nakanishi, Shima; Licht, Konstantin; Rosenberg, Laura H.; Li, Lin; Feng, Yangbo; Cameron, Michael D.; Duckett, Derek R.; Cleveland, John L.; Roush, William R.
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 15 p. 4374 - 4380
