1-(4-硝基苯基)-1H-吡咯合成路线 (共 17 条)
反应条件
tungstophosphoric acid supported on silica gel 30 h; Microwave irradiationNeat (no solvent);
参考文献
Jafari; Mahmoudi; Mirjalili
Journal of the Iranian Chemical Society, 2011 , vol. 8, # 3 p. 851 - 856
反应条件
copper(l) iodide; N-(acetylamino-phenyl-methyl)-acetamide; sodium methylate in dimethyl sulfoxide T=110°C; 12 h;
参考文献
Arundhathi, Racha; Kumar, Desitti Chaitanya; Sreedhar, Bojja
European Journal of Organic Chemistry, 2010 , # 19 p. 3621 - 3630
反应条件
copper(l) iodide; caesium carbonate in dimethyl sulfoxide T=110°C; 24 h;
参考文献
Reddy, V. Prakash; Kumar, A. Vijay; Rao, K. Rama
Tetrahedron Letters, 2011 , vol. 52, # 7 p. 777 - 780
反应条件
KNO2; copper(II) bis(trifluoromethanesulfonate) in dimethyl sulfoxide T=130°C; 48 h; Inert atmosphereSealed tube; regioselective reaction;
参考文献
Amal Joseph; Priyadarshini; Lakshmi Kantam; Maheswaran
Tetrahedron Letters, 2012 , vol. 53, # 12 p. 1511 - 1513
反应条件
potassium carbonate; trans-1,2-diaminocyclohexane-based copper(II) complex in N,N-dimethyl-formamide T=110°C; 1.5 h;
参考文献
Kantam, M. Lakshmi; Ramani; Chakrapani
Synthetic Communications, 2008 , vol. 38, # 4 p. 626 - 636
反应条件
copper(II) ferrite; potassium tert-butylate in N,N-dimethyl-formamide T=155°C; 24 h; Inert atmosphere;
参考文献
Panda, Niranjan; Jena, Ashis Kumar; Mohapatra, Sasmita; Rout, Smruti Ranjan
Tetrahedron Letters, 2011 , vol. 52, # 16 p. 1924 - 1927
反应条件
tris-(dibenzylideneacetone)dipalladium(0); t-Bu Brett Phos; TDA; sodium nitrite in tert-butyl alcohol T=130°C; 24 h; regioselective reaction;
参考文献
Fors, Brett P.; Buchwald, Stephen L.
Journal of the American Chemical Society, 2009 , vol. 131, # 36 p. 12898 - 12899
反应条件
copper; caesium carbonate in acetonitrile 10 h; RefluxInert atmosphere;
参考文献
Zhu, Rui; Xing, Lixin; Wang, Xinyan; Cheng, Chuanjie; Su, Deyong; Hu, Yuefei
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 9 p. 1253 - 1257
反应条件
bis(tricyclohexylphosphine)benzylidene ruthenium(IV) dichloride in dichloromethane T=100°C; 0.166667 h; microwave irradiation;
参考文献
Yang, Qian; Li, Xin-Yong; Wu, Hong; Xiao, Wen-Jing
Tetrahedron Letters, 2006 , vol. 47, # 23 p. 3893 - 3896
反应条件
sodium tetrahydroborate; sulfuric acid; water in tetrahydrofuran; methanol T=10 - 20°C; 1.5 h; Yield given;
参考文献
Verardo, Giancarlo; Dolce, Anna; Toniutti, Nicoletta
Synthesis, 1999 , # 1 p. 74 - 79