Behandlung des Produkts mit Ammoniak;

1.1: ammonium hydroxide / toluene; water; tetrahydrofuran / 2 h / -10 °C / Reflux 1.2: pH 4 2.1: ammonium hydroxide; (NH4)2CO3; copper(II) sulfate / water / 72 h / 118 °C / Autoclave; Industry scale 3.1: hydrogen / palladium 10 on activated carbon / tetrahydrofuran; methanol / 23 °C / 2585.81 Torr / Industry scale; Autoclave 4.1: pyridine / dichloromethane / 0 - 23 °C / Industry scale 5.1: tetrahydrofuran / 1 h / 0 - 23 °C / Industry scale 6.1: sodium hydroxide; water / 30 h / 23 °C / Industry scale 6.2: 0 °C / Industry scale View Scheme

1: HI 2: 79 percent / glucose, NaOH / methanol; H2O / 20 h / 50 °C 3: 65 percent / Zn / 4 h / Heating View Scheme

1: HI 2: 79 percent / glucose, NaOH / methanol; H2O / 20 h / 50 °C View Scheme

sodium hydroxide

1: ammonia / water / 1 h / 20 °C 2: ammonia; (NH4)2CO3; copper(II) sulfate / water / Reflux View Scheme

1: HI 2: 79 percent / glucose, NaOH / methanol; H2O / 20 h / 50 °C 3: 93 percent / Zn, aq. HCl / acetic acid / 1.5 h / Heating View Scheme

d-N,a-dimethylphenethylamine; sodium sulfite

暂无反应条件数据

1: 90 percent / Ph4PBr, KF / tetrahydrothiophene 1,1-dioxide / 16 h / 130 - 140 °C 2: KF, PPh4Br / tetrahydrothiophene 1,1-dioxide; toluene / 210 °C / 300 Torr View Scheme