1.1: NaH / 1,2-dimethoxy-ethane / 0.25 h / 0 °C 1.2: 1,2-dimethoxy-ethane / 0.25 h / 0 °C 2.1: DIBAL / toluene / 0.33 h / 0 °C 3.1: MnO2 / CH2Cl2 / 2 h / 20 °C View Scheme
参考文献
Park, Jungmin; Yun, Jihee; Kim, Jaehyun; Jang, Dong-Jin; Park, Cheol Ho; Lee, Kooyeon
Synthetic Communications, 2014 , vol. 44, # 13 p. 1924 - 1929
1.1: n-butyllithium / diethyl ether / 1 h / -78 °C 1.2: diethyl ether / 2.5 h / 20 °C 2.1: 0.61 g / oxalyl chloride; DMSO; triethylamine / CH2Cl2 / 1 h / 20 °C View Scheme
参考文献
Mills, Nancy S.; Tirla, Cornelia; Benish, Michele A.; Rakowitz, Amber J.; Bebell, Lisa M.; Hurd, Caroline M. M.; Bria, Anna L. M.
Journal of Organic Chemistry, 2005 , vol. 70, # 26 p. 10709 - 10716
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Journal of Medicinal Chemistry, 2007 , vol. 50, # 1 p. 65 - 73
