(4-甲氧基羰基甲基)苯硼酸合成路线 (共 3 条)
反应条件
1: With bis-(2-hydroxy-ethyl)-amine in diethyl ether; isopropyl alcohol 2: With hydrogenchloride in tetrahydrofuran; water T=20°C; Further stages.;
参考文献
Wang, You-Chu; Georghiou, Paris E.
Organic Letters, 2002 , vol. 4, # 16 p. 2675 - 2678
反应条件
1.1: 98 percent / 2,6-lutidine / CH2Cl2 / -40 °C 2.1: 85 percent / potassium acetate; PdCl2(dppf) / dioxane / 80 °C 3.1: diethanolamine / propan-2-ol; diethyl ether 3.2: hydrochloric acid / H2O; tetrahydrofuran / 20 °C View Scheme
参考文献
Wang, You-Chu; Georghiou, Paris E.
Organic Letters, 2002 , vol. 4, # 16 p. 2675 - 2678
反应条件
1.1: 85 percent / potassium acetate; PdCl2(dppf) / dioxane / 80 °C 2.1: diethanolamine / propan-2-ol; diethyl ether 2.2: hydrochloric acid / H2O; tetrahydrofuran / 20 °C View Scheme
参考文献
Wang, You-Chu; Georghiou, Paris E.
Organic Letters, 2002 , vol. 4, # 16 p. 2675 - 2678