4,4’-二(溴甲基)二苯醚合成路线 (共 7 条)
反应条件
phosphorus tribromide in tetrahydrofuran; toluene T=20°C;
参考文献
Gibson, Harry W.; Wang, Hong; Niu, Zhenbin; Slebodnick, Carla; Zhakharov, Lev N.; Rheingold, Arnold L.
Macromolecules, 2012 , vol. 45, # 3 p. 1270 - 1280
反应条件
bromine; ethylene dibromide; dibenzoyl peroxide Irradiation.Sonnenlicht;
参考文献
Schrader, Thomas
Chemistry - A European Journal, 1997 , vol. 3, # 9 p. 1537 - 1541
反应条件
1: 91 percent / LiAlH4 / tetrahydrofuran / 72 h / 0 °C 2: 69 percent / PPh3; NBS / tetrahydrofuran / 96 h / 20 °C View Scheme
参考文献
Shimizu, Linda S.; Hughes, Andrew D.; Smith, Mark D.; Davis, Matthew J.; Zhang, B. Paul; Zur Loye, Hans-Conrad; Shimizu, Ken D.
Journal of the American Chemical Society, 2003 , vol. 125, # 49 p. 14972 - 14973
反应条件
1: Zn, AcOH, aq. CuSO4 2: SO2Cl2, (PhCO)2O2 View Scheme
参考文献
Golden,J.H.
Journal of the Chemical Society, 1961 , p. 1604 - 1610
反应条件
1: Zn, AcOH, aq. CuSO4 2: aq. KMnO4 View Scheme
参考文献
Golden,J.H.
Journal of the Chemical Society, 1961 , p. 1604 - 1610
反应条件
copper(II) sulfate; acetic acid; zinc
参考文献
Journal of the Chemical Society, , p. 1604 - 1610
反应条件
chloroform Erhitzen des Reaktionsprodukts mit wss. Essigsaeure und anschliessend mit wss. HCl;
参考文献
Ito; Shibanuma
Pharmaceutical Bulletin, 1957 , vol. 5, p. 619