(-)-α-新丁香三环烯合成路线 （共 11 条）
反应条件
sulfuric acid in diethyl ether 72 h; Ambient temperature; Further byproducts given;
参考文献
Fitjer, Lutz; Malich, Andreas; Paschke, Carola; Kluge, Sabine; Gerke, Ralf; Rissom, Beate; Weiser, Joerg; Noltemeyer, Mathias
Journal of the American Chemical Society, 1995 , vol. 117, # 36 p. 9180 - 9189
反应条件
sulfuric acid in diethyl ether T=20°C; 5 h;
参考文献
Khomenko, T. M.; Korchagina, D. V.; Gatilov, Yu. V.; Bagrayanskaya, I. Yu.; Rybalova, T. V.; et al.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, # 3.2 p. 493 - 516
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, # 3 p. 570 - 599
反应条件
pyridine; thionyl chloride 0.166667 h; Title compound not separated from byproducts;
参考文献
Fitjer, Lutz; Malich, Andreas; Paschke, Carola; Kluge, Sabine; Gerke, Ralf; Rissom, Beate; Weiser, Joerg; Noltemeyer, Mathias
Journal of the American Chemical Society, 1995 , vol. 117, # 36 p. 9180 - 9189
反应条件
1: 4 mg / diethyl ether / 1 h / Heating 2: cc. H2SO4 / diethyl ether / 1.) 0 deg C, 20 min; 2.) 30 min, RT View Scheme
参考文献
Iwabuchi; Yoshikura; Ikawa; Kamisako
Chemical and pharmaceutical bulletin, 1987 , vol. 35, # 5 p. 1975 - 1981
反应条件
sulfuric acid in diethyl ether 1.) 0 deg C, 20 min; 2.) 30 min, RT;
参考文献
Iwabuchi; Yoshikura; Ikawa; Kamisako
Chemical and pharmaceutical bulletin, 1987 , vol. 35, # 5 p. 1975 - 1981
参考文献
Parker,W. et al.
Journal of the Chemical Society [Section] C: Organic, 1969 , p. 2634 - 2643
参考文献
McKillop,T.F.W. et al.
Journal of the Chemical Society [Section] C: Organic, 1971 , p. 3375 - 3384
反应条件
1: Py 2: (i) (pyrolysis), (ii) H2, Pd-C 4: H2SO4 View Scheme
参考文献
McKillop,T.F.W. et al.
Journal of the Chemical Society [Section] C: Organic, 1971 , p. 3375 - 3384
反应条件
1: (i) (pyrolysis), (ii) H2, Pd-C 3: H2SO4 View Scheme
参考文献
McKillop,T.F.W. et al.
Journal of the Chemical Society [Section] C: Organic, 1971 , p. 3375 - 3384
反应条件
2: H2SO4 View Scheme
参考文献
McKillop,T.F.W. et al.
Journal of the Chemical Society [Section] C: Organic, 1971 , p. 3375 - 3384
