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乙二醇
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63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
N6-苯甲酰基腺苷
合成路线
（共 31 条）
184229-68-3
→
反应条件
4546-55-8
N6-苯甲酰基腺苷
反应条件
hydrogen; palladium in ethanol T=45°C; P=760 Torr; 9 h;
参考文献
Henningfeld, Kristine A.; Arslan, Tuncer; Hecht, Sidney M.
Journal of the American Chemical Society, 1996 , vol. 118, # 47 p. 11701 - 11714
98-88-4
苯甲酰氯
+
58-61-7
腺苷
→
反应条件
4546-55-8
N6-苯甲酰基腺苷
反应条件
in pyridine T=0°C;
参考文献
Cole, Andrew G.; Gani, David
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 21 p. 2685 - 2694
98-88-4
苯甲酰氯
→
反应条件
4546-55-8
N6-苯甲酰基腺苷
反应条件
1: 9-beta-D-arabinofuranosyladenine With pyridine; chloro-trimethyl-silane 0.25 h; 2: benzoyl chloride T=20°C; 2 h; 3: With ammonia; water T=0 - 20°C; 0.583333 h;
参考文献
MILLENNIUM PHARMACEUTICALS, INC.
Patent: WO2006/84281 A1, 2006 ;
Location in patent: Page/Page column 123-124 ;
14686-89-6
二丙酮-D-葡萄糖
→
反应条件
4546-55-8
N6-苯甲酰基腺苷
反应条件
1: sodium hydride / dimethylformamide / 1 h / Ambient temperature 2: acetic acid, p-toluenesulfonic acid monohydrate / 1 h / Heating 3: 71 percent / trimethylsilyl trifluoromethanesulfonate / acetonitrile / 12 h / 55 °C 4: 86 percent / ethanolic NaOH / pyridine / 0.17 h / Ambient temperature 5: NaIO4 / tetrahydrofuran; H2O / 2 h / Ambient temperature 6: NaBH4 / methanol / 0.5 h / Ambient temperature 7: 68 percent / H2 / Pd black / ethanol / 9 h / 45 °C / 760 Torr View Scheme
参考文献
Henningfeld, Kristine A.; Arslan, Tuncer; Hecht, Sidney M.
Journal of the American Chemical Society, 1996 , vol. 118, # 47 p. 11701 - 11714
22331-21-1
3-O-苄基-1,2:5,6-双-O-异丙亚基-alpha-D-呋喃半乳糖
→
反应条件
4546-55-8
N6-苯甲酰基腺苷
反应条件
1: acetic acid, p-toluenesulfonic acid monohydrate / 1 h / Heating 2: 71 percent / trimethylsilyl trifluoromethanesulfonate / acetonitrile / 12 h / 55 °C 3: 86 percent / ethanolic NaOH / pyridine / 0.17 h / Ambient temperature 4: NaIO4 / tetrahydrofuran; H2O / 2 h / Ambient temperature 5: NaBH4 / methanol / 0.5 h / Ambient temperature 6: 68 percent / H2 / Pd black / ethanol / 9 h / 45 °C / 760 Torr View Scheme
参考文献
Henningfeld, Kristine A.; Arslan, Tuncer; Hecht, Sidney M.
Journal of the American Chemical Society, 1996 , vol. 118, # 47 p. 11701 - 11714
184229-59-2
→
反应条件
4546-55-8
N6-苯甲酰基腺苷
反应条件
1: 71 percent / trimethylsilyl trifluoromethanesulfonate / acetonitrile / 12 h / 55 °C 2: 86 percent / ethanolic NaOH / pyridine / 0.17 h / Ambient temperature 3: NaIO4 / tetrahydrofuran; H2O / 2 h / Ambient temperature 4: NaBH4 / methanol / 0.5 h / Ambient temperature 5: 68 percent / H2 / Pd black / ethanol / 9 h / 45 °C / 760 Torr View Scheme
参考文献
Henningfeld, Kristine A.; Arslan, Tuncer; Hecht, Sidney M.
Journal of the American Chemical Society, 1996 , vol. 118, # 47 p. 11701 - 11714
184229-61-6
→
反应条件
4546-55-8
N6-苯甲酰基腺苷
反应条件
1: NaIO4 / tetrahydrofuran; H2O / 2 h / Ambient temperature 2: NaBH4 / methanol / 0.5 h / Ambient temperature 3: 68 percent / H2 / Pd black / ethanol / 9 h / 45 °C / 760 Torr View Scheme
参考文献
Henningfeld, Kristine A.; Arslan, Tuncer; Hecht, Sidney M.
Journal of the American Chemical Society, 1996 , vol. 118, # 47 p. 11701 - 11714
184229-60-5
→
反应条件
4546-55-8
N6-苯甲酰基腺苷
反应条件
1: 86 percent / ethanolic NaOH / pyridine / 0.17 h / Ambient temperature 2: NaIO4 / tetrahydrofuran; H2O / 2 h / Ambient temperature 3: NaBH4 / methanol / 0.5 h / Ambient temperature 4: 68 percent / H2 / Pd black / ethanol / 9 h / 45 °C / 760 Torr View Scheme
参考文献
Henningfeld, Kristine A.; Arslan, Tuncer; Hecht, Sidney M.
Journal of the American Chemical Society, 1996 , vol. 118, # 47 p. 11701 - 11714
118684-36-9
→
反应条件
4546-55-8
N6-苯甲酰基腺苷
反应条件
ammonium hydroxide in pyridine T=25°C; 0.25 h; Yield given;
参考文献
Cui, Zhiyong; Zhang, Lei; Zhang, Biliang
Tetrahedron Letters, 2001 , vol. 42, # 4 p. 561 - 563
58-61-7
腺苷
→
反应条件
4546-55-8
N6-苯甲酰基腺苷
反应条件
1: pyridine / 0.5 h / 20 °C 2: pyridine / 2 h / 20 °C 3: aq. NH4OH / 0.25 h / 20 °C View Scheme
参考文献
Zhu, Xue-Feng; Williams Jr., Howard J.; Scott, A. Ian
Synthetic Communications, 2003 , vol. 33, # 7 p. 1233 - 1243
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