N-苯甲酰基-2’-脱氧腺苷合成路线 （共 27 条）
参考文献
Gilead Sciences, Inc.
Patent: US5672697 A1, 1997 ;
反应条件
1: pyridine / 1 h / Ambient temperature 2: NH3 / pyridine; H2O / 0.5 h View Scheme
参考文献
Grotli, Morten; Eritja, Ramon; Sproat, Brian
Tetrahedron, 1997 , vol. 53, # 33 p. 11317 - 11346
反应条件
diisobutyl-aluminum chloride in dichloromethane Ambient temperature; Yield given;
参考文献
Koester, H.; Sinha, N. D.
Tetrahedron Letters, 1982 , vol. 23, # 26 p. 2641 - 2644
反应条件
zinc dibromide in dichloromethane 0.0833333 h; Ambient temperature;
参考文献
Kohli, V.; Bloecker, H.; Koester, H.
Tetrahedron Letters, 1980 , vol. 21, p. 2683 - 2686
反应条件
in methanol UV-irradiation; Quantum yield; Wavelength;
参考文献
Woell, Dominik; Smirnova, Julia; Galetskaya, Marina; Prykota, Tamara; Buehler, Jochen; Stengele, Klaus-Peter; Pfleiderer, Wolfgang; Steiner, Ulrich E.
Chemistry - A European Journal, 2008 , vol. 14, # 21 p. 6490 - 6497
反应条件
1: 82 percent / pyridine / 24 h / -20 °C 2: 51 percent / CH3ONa / methanol / 2 h / Heating 3: 51 percent / triethyl phosphite / acetonitrile / 10 h / Irradiation 4: 79 percent / imidazole / dimethylformamide / 20 h / Ambient temperature 5: 87 percent / SeO2 / dioxane / 1 h / Heating View Scheme
参考文献
Romieu, Anthony; Gasparutto, Didier; Molko, Didier; Cadet, Jean
Journal of Organic Chemistry, 1998 , vol. 63, # 15 p. 5245 - 5249
反应条件
ethylenediamine T=40°C; 20 h;
参考文献
Tetrahedron Letters, , vol. 22, p. 991 - 994
反应条件
1: With 1H-tetrazole; long chain alkylamine controlled pore glass; 3-keto-2H,3H-1,2-benzisothiazole 1,1-dioxide in acetonitrile 2: With ammonia T=25°C; P=7500.6 Torr; 1.5 h;
参考文献
Wilk, Andrzej; Chmielewski, Marcin K.; Grajkowski, Andrzej; Phillips, Lawrence R.; Beaucage, Serge L.
Tetrahedron Letters, 2001 , vol. 42, # 33 p. 5635 - 5639
反应条件
1: aq. NH3 / 5.5 h / 55 °C 2: 92 percent / H2O / 12 h / 30 °C View Scheme
参考文献
Chirakul; Litzer; Sigurdsson
Nucleosides, Nucleotides and Nucleic Acids, 2001 , vol. 20, # 12 p. 1903 - 1913
参考文献
Tetrahedron Letters, , vol. 33, # 48 p. 7319 - 7323
