Phillips; Shapiro
Journal of the Chemical Society, 1942 , p. 584
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Binz; Maier-Bode
Angewandte Chemie, 1936 , vol. 49, p. 486,488
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Raeth
Justus Liebigs Annalen der Chemie, 1931 , vol. 487, p. 105,115
1: 83 percent / CsF / various solvent(s) / 18 h / 130 °C 2: 94 percent / H2, Na2SO4 / 5percent Pd/C / toluene 3: 88 percent / 1,2-dichloro-ethane / 16 h / Heating 4: 47 percent / TMEDA, BuLi / diethyl ether; hexane / 1.) -40 deg C, 16 h, 2.) -40 deg C to r.t., 1 h 5: 94 percent / H2O, TFA / CH2Cl2 / 14 h / Ambient temperature 6: 89 percent / 2-methoxy-ethanol / 12 h / Heating View Scheme
参考文献
Rewcastle, Gordon W.; Denny, William A.; Winters, R. Thomas; Colbry, Norman L.; Showalter, H. D. Hollis
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 18 p. 2221 - 2226
1: 84 percent / KF / dimethylsulfoxide / 18 h / 70 °C 2: 70 percent / H2 / Raney Ni / ethyl acetate 3: 96 percent / 2-methyl-propan-2-ol / 4 h / 40 °C View Scheme
参考文献
Rewcastle, Gordon W.; Denny, William A.; Winters, R. Thomas; Colbry, Norman L.; Showalter, H. D. Hollis
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 18 p. 2221 - 2226