4-氯-2-硝基二苯硫醚合成路线 （共 10 条）
反应条件
sodium hydroxide in methanol T=20°C; 4 h;
参考文献
ALLERGAN, INC.; YUAN, HAIQING; BEARD, RICHARD L.; LIU, XIAOXIA; DONELLO, JOHN E.; VISWANATH, VEENA; GARST, MICHAEL E.
Patent: US2013/231338 A1, 2013 ;
Location in patent: Paragraph 0341; 0342; 0343 ;
反应条件
ammonium acetate in ethanol 48 h; Heating;
参考文献
Bonnet, Beatrice; Soullez, David; Davioud-Charvet, Elisabeth; Landry, Valerie; Horvath, Dragos; Sergheraert, Christian
Bioorganic and Medicinal Chemistry, 1997 , vol. 5, # 7 p. 1249 - 1256
反应条件
sodium hydroxide in ethanol; water 2 h; Reflux;
参考文献
Catarinella, Mario; Gruener, Tamara; Strittmatter, Tobias; Marx, Andreas; Mayer, Thomas U.
Angewandte Chemie - International Edition, 2009 , vol. 48, # 48 p. 9072 - 9076
反应条件
sodium hydroxide; ethanol Heating;
参考文献
Lambert; Bertin; Lacoste; Volland; Krick; Furet; Botrel; Guenot
Journal of Mass Spectrometry, 1998 , vol. 33, # 3 p. 242 - 249
参考文献
Loudon
Journal of the Chemical Society, 1939 , p. 902,904
参考文献
Loudon
Journal of the Chemical Society, 1939 , p. 902,904
反应条件
isopropyl-benzene; triethyl phosphite Heating;
参考文献
Cadogan,J.I.G. et al.
Journal of the Chemical Society [Section] C: Organic, 1970 , p. 2437 - 2441
反应条件
dihydrogen peroxide; acetic acid
参考文献
Grundon,M.F. et al.
Journal of the Chemical Society [Section] B: Physical Organic, 1966 , p. 260 - 266
反应条件
hydrogenchloride; iron in ethanol
1 h; Heating;
参考文献
ALLERGAN, INC.; YUAN, HAIQING; BEARD, RICHARD L.; LIU, XIAOXIA; DONELLO, JOHN E.; VISWANATH, VEENA; GARST, MICHAEL E.
Patent: US2013/231338 A1, 2013 ;
Location in patent: Paragraph 0344; 0345; 0346 ;
反应条件
1: aq. H2O2 / acetic acid / Heating
2: H2 / Pt / tetrahydrofuran
View Scheme
参考文献
Grundon,M.F. et al.
Journal of the Chemical Society [Section] B: Physical Organic, 1966 , p. 260 - 266
