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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-碘三氟甲苯
合成路线
（共 220 条）
455-13-0
4-碘三氟甲苯
→
反应条件
402-54-0
4-硝基三氟甲苯
反应条件
copper; TBANO2; N-methyl-2-(methylamino)ethylamine in N,N-dimethyl-formamide T=110°C; 0.25 h; Inert atmosphereMicrowave irradiation;
参考文献
LaBeaume, Paul; Placzek, Michael; Daniels, Mathew; Kendrick, Ian; Ng, Patrick; McNeel, Melissa; Afroze, Roushan; Alexander, Abigail; Thomas, Rhiannon; Kallmerten, Amy E.; Jones, Graham B.
Tetrahedron Letters, 2010 , vol. 51, # 14 p. 1906 - 1909
455-13-0
4-碘三氟甲苯
+
78599-06-1
→
反应条件
402-50-6
4-(三氟甲基)苯乙烯
反应条件
tetrabutyl ammonium fluoride; palladium diacetate in tetrahydrofuran T=25°C; 0.5 h;
参考文献
Hosoi, Kazushi; Nozaki, Kyoko; Hiyama, Tamejiro
Chemistry Letters, 2002 , # 2 p. 138 - 139
455-13-0
4-碘三氟甲苯
+
4627-10-5
4,4,6-三甲基-2-乙烯基-1,3,2-二氧杂硼烷
→
反应条件
402-50-6
4-(三氟甲基)苯乙烯
反应条件
silver(l) oxide; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=67°C; Suzuki-Miyaura reaction; 24 h;
参考文献
Lightfoot, Andrew P.; Twiddle, Steven J. R.; Whiting, Andrew
Synlett, 2005 , # 3 art. no. D32204ST, p. 529 - 531
54509-73-8
+
455-13-0
4-碘三氟甲苯
→
反应条件
402-50-6
4-(三氟甲基)苯乙烯
反应条件
N,N-dicyclohexylmethylamine; palladium diacetate; tetra-(n-butyl)ammonium iodide; [(t-Bu)3PH]BF4 in methanol; toluene T=130°C; Heck Reaction; P=7500.75 Torr; 0.333333 h; Reagent/catalystSolventTemperature;
参考文献
Bourne, Samuel L.; O'Brien, Matthew; Kasinathan, Sivarajan; Koos, Peter; Tolstoy, Paeivi; Hu, Dennis X.; Bates, Roderick W.; Martin, Benjamin; Schenkel, Berthold; Ley, Steven V.
ChemCatChem, 2013 , vol. 5, # 1 p. 159 - 172
455-13-0
4-碘三氟甲苯
+
7486-35-3
三丁基乙烯基锡
→
反应条件
402-50-6
4-(三氟甲基)苯乙烯
反应条件
diisobutylaluminium hydride; bis(acetylacetonate)nickel(II); triphenylphosphine in ethylene glycol dimethyl ether; hexane T=50°C; 20 h;
参考文献
Shirakawa, Eiji; Yamasaki, Kenji; Hiyama, Tamejiro
Synthesis, 1998 , # 10 p. 1544 - 1549
288-13-1
吡唑
+
455-13-0
4-碘三氟甲苯
→
反应条件
207797-05-5
1-(4-(三氟甲基)苯基)-1H-吡唑
反应条件
copper(l) iodide; manganese(II) fluoride; (1R,2R)-(-)-trans-1,2-diaminocyclohexane; potassium hydroxide in water T=60°C; 24 h;
参考文献
Teo, Yong-Chua; Yong, Fui-Fong; Lim, Gina Shiyun
Tetrahedron Letters, 2011 , vol. 52, # 52 p. 7171 - 7174
110-86-1
吡啶
+
455-13-0
4-碘三氟甲苯
→
反应条件
203065-88-7
2-[4-(三氟甲基)苯基]吡啶
+
220000-88-4
4-(4-三氟甲基苯基)吡啶
+
426823-25-8
3-[4-(三氟甲基）苯基]吡啶
反应条件
Br(1-)*C18H28N3(1+); sodium t-butanolate T=110°C; 48 h; Inert atmosphere;
参考文献
Chen, Wen-Ching; Hsu, Yu-Chen; Shih, Wei-Chun; Lee, Ching-Yu; Chuang, Wen-Han; Tsai, Yi-Fang; Chen, Peter Ping-Yu; Ong, Tiow-Gan
Chemical Communications, 2012 , vol. 48, # 53 p. 6702 - 6704
212317-59-4
+
455-13-0
4-碘三氟甲苯
→
反应条件
635702-14-6
+
624-49-7
富马酸二甲酯
反应条件
in chloroform-d1 Pd:ligand =1:5-1:10, at 25°C; not isolated, detected by NMR;
参考文献
European Journal of Inorganic Chemistry, , # 4 p. 732 - 742
635702-08-8
+
455-13-0
4-碘三氟甲苯
→
反应条件
635702-17-9
+
624-49-7
富马酸二甲酯
反应条件
in acetonitrile Kinetics; at 45°C; not isolated, detected by NMR;
参考文献
European Journal of Inorganic Chemistry, , # 4 p. 732 - 742
54509-73-8
+
696-62-8
4-碘苯甲醚
+
455-13-0
4-碘三氟甲苯
→
反应条件
637-69-4
4-甲氧基苯乙烯
+
40473-89-0
反应条件
1: ethene; para-iodoanisole With palladium diacetate; tetra-(n-butyl)ammonium iodide; triethylamine; 2-dicyclohexylphosphino-1,1'-biphenyl in N,N-dimethyl-formamide; toluene T=120°C; Mizoroki-Heck coupling; P=11251.1 Torr; 0.333333 h; 2: 4-trifluoromethyl-1-iodobenzene With palladium diacetate; tetra-(n-butyl)ammonium iodide; triethylamine; 2-dicyclohexylphosphino-1,1'-biphenyl in N,N-dimethyl-formamide; toluene T=120°C; Heck reaction; P=15001.5 Torr;
参考文献
Bourne, Samuel L.; Koos, Peter; Obrien, Matthew; Martin, Benjamin; Schenkel, Berthold; Baxendale, Ian R.; Ley, Steven V.
Synlett, 2011 , # 18 p. 2643 - 2647
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