1-氟-4-(三甲基硅基)苯合成路线 （共 39 条）
反应条件
boron trifluoride-methanol; fluorine in methanol; dichloromethane; monofluoro-trichloromethane T=-78°C; 5 h; Title compound not separated from byproducts;
参考文献
Journal of Fluorine Chemistry, , vol. 88, # 2 p. 179 - 184
反应条件
Stirring of silane with a slurry of Pb(OAc)4 in excess of BF3*Et2O overnight at room temp.; GC anal.;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 15 p. 1065 - 1066
反应条件
Montmorillonite KSF in water T=20°C;
参考文献
Zafrani, Yossi; Gershonov, Eytan; Columbus, Ishay
Journal of Organic Chemistry, 2007 , vol. 72, # 18 p. 7014 - 7017
反应条件
Ph3PAuOTs; camphor-10-sulfonic acid; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in methanol; chloroform T=65°C;
参考文献
Science (Washington, DC, United States), , vol. 337, # 6102 p. 1644 - 1648,5
反应条件
water; nitric acid; acetic anhydride T=50°C; 27 h;
参考文献
Journal of Fluorine Chemistry, , vol. 92, # 1 p. 27 - 32
反应条件
Ph3PAuOTs; [bis(acetoxy)iodo]benzene; camphor-10-sulfonic acid in methanol; chloroform
T=20°C;
参考文献
Ball, Liam T.; Lloyd-Jones, Guy C.; Russell, Christopher A.
Science (Washington, DC, United States), 2012 , vol. 337, # 6102 p. 1644 - 1648,5
反应条件
Ph3PAuOTs; [bis(acetoxy)iodo]benzene; camphor-10-sulfonic acid in methanol; chloroform
T=20°C;
参考文献
Ball, Liam T.; Lloyd-Jones, Guy C.; Russell, Christopher A.
Science (Washington, DC, United States), 2012 , vol. 337, # 6102 p. 1644 - 1648,5
反应条件
copper dichloride; palladium dichloride in 1,2-dichloro-ethane
T=80°C; 16 h;
参考文献
Funaki, Kenji; Kawai, Hiroshi; Sato, Tetsuo; Oi, Shuichi
Chemistry Letters, 2011 , vol. 40, # 9 p. 1050 - 1052
反应条件
Ph3PAuOTs; [bis(acetoxy)iodo]benzene; camphor-10-sulfonic acid in methanol; chloroform
T=20°C;
参考文献
Ball, Liam T.; Lloyd-Jones, Guy C.; Russell, Christopher A.
Science (Washington, DC, United States), 2012 , vol. 337, # 6102 p. 1644 - 1648,5
