1: With 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; tert-butylhypochlorite in dichloromethane T=20°C; 1 h; Inert atmosphere; 2: With ammonia; iodine in dichloromethane; water T=20°C; 2 h; Inert atmosphere;
tetra-N-butylammonium azide in acetonitrile T=25.5°C; in the dark; Kinetics;
参考文献
Moss, Robert A.; Terpinski, Jacek; Cox, D. Phillip; Denneey, Dorothy Z.; Krogh-Jespersen, Karsten
Journal of the American Chemical Society, 1985 , vol. 107, # 9 p. 2743 - 2748