3-氨基-5-甲硫基-1H-1,2,4-三唑合成路线 （共 33 条）
反应条件
sodium hydride 1.) DMF, 0 deg C, 1 h, 2.) DMF, 60 deg C, 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Trinka, Peter; Reiter, Jozsef
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 4 p. 1359 - 1372
反应条件
sodium hydride 1.) DMF, 0 deg C, 1 h, 2.) DMF, 60 deg C, 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Trinka, Peter; Reiter, Jozsef
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 4 p. 1359 - 1372
反应条件
sodium hydride 1.) DMF, 0 deg C, 1 h, 2.) DMF, 60 deg C, 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Heterocyclic Chemistry, , vol. 32, # 4 p. 1359 - 1372
反应条件
sodium hydride 1.) DMF, 0 deg C, 1 h, 2.) DMF, 60 deg C, 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Heterocyclic Chemistry, , vol. 32, # 4 p. 1359 - 1372
反应条件
potassium hydroxide
1.) DMF, 80 deg C, 4 h 2.) 25 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Pongo, Laszlo; Reiter, Jozsef; Barkoczy, Jozsef; Sohar, Pal; Pallagi, Istvan
Journal of Heterocyclic Chemistry, 1990 , vol. 27, # 5 p. 1249 - 1257
反应条件
hydrogenchloride
T=20 - 25°C; 0.5 h;
参考文献
Rusinov, V. L.; Pilicheva, T. L.; Chupakhin, O. N.; Kovalev, G. V.; Komina, E. R.
Pharmaceutical Chemistry Journal, 1986 , vol. 20, # 8 p. 550 - 554
Khimiko-Farmatsevticheskii Zhurnal, 1986 , vol. 20, # 8 p. 947 - 952
反应条件
in N,N-dimethyl-formamide
60 h; Ambient temperature;
参考文献
Naito, Youichiro; Akahoshi, Fumihiko; Takeda, Shinji; Okada, Takehiro; Kajii, Masahiko; Nishimura, Hiroko; Sugiura, Masanori; Fukaya, Chikara; Kagitani, Yoshio
Journal of Medicinal Chemistry, 1996 , vol. 39, # 15 p. 3019 - 3029
反应条件
sodium hydride
1) toluene, DMF, 0 deg C, 0.5 h, 2) 0 deg C, 3 h, r.t.; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Reiter, J.; Somorai, T.; Dvortsak, P.; Bujtas, Gy.
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 385 - 394
反应条件
sodium hydride
1) toluene, DMF, 0 deg C, 0.5 h, 2) 0 deg C, 3 h, r.t.; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Reiter, J.; Somorai, T.; Dvortsak, P.; Bujtas, Gy.
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 385 - 394
反应条件
sodium hydride
1) toluene, DMF, 0 deg C, 0.5 h, 2) 0 deg C, 3 h, r.t.; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Reiter, J.; Somorai, T.; Dvortsak, P.; Bujtas, Gy.
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 385 - 394
