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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
二苯基磷氧
合成路线
（共 390 条）
845821-95-6
+
4559-70-0
二苯基磷氧
→
反应条件
845821-92-3
[6,6-二(二苯基膦基)-2,4-环己二烯-1-基](苯基)甲酮
反应条件
N-ethyl-N,N-diisopropylamine; palladium diacetate; 1,4-di(diphenylphosphino)-butane in dimethyl sulfoxide T=100°C; 18 h; Product distribution / selectivity;
参考文献
Takasago International Corporation
Patent: EP1661903 A1, 2006 ;
Location in patent: Page/Page column 64 ;
696-62-8
4-碘苯甲醚
+
4559-70-0
二苯基磷氧
→
反应条件
896-89-9
对茴香基二苯基膦
反应条件
1: diphenylphosphine oxide With cupric triflate; 1,1,3,3-tetramethyldisiloxane in toluene T=100°C; 10 h; Inert atmosphere; 2: para-iodoanisole With caesium carbonate; N-methyl-2-(methylamino)ethylamine in toluene T=20 - 110°C; Inert atmosphere;
参考文献
Li, Yuehui; Das, Shoubhik; Zhou, Shaolin; Junge, Kathrin; Beller, Matthias
Journal of the American Chemical Society, 2012 , vol. 134, # 23 p. 9727 - 9732
4559-70-0
二苯基磷氧
+
614-47-1
反式-查耳酮
→
反应条件
912-28-7
反应条件
T=130°C; phospha-Michael addition; 0.583333 h; Neat (no solvent)Inert atmosphereMicrowave irradiation;
参考文献
Lenker, Heather K.; Richard, Marcia E.; Reese, Kyle P.; Carter, Anthony F.; Zawisky, Jason D.; Winter, Eric F.; Bergeron, Timothy W.; Guydon, Krysta S.; Stockland, Robert A.
Journal of Organic Chemistry, 2012 , vol. 77, # 3 p. 1378 - 1385
139139-80-3
+
4559-70-0
二苯基磷氧
→
反应条件
91239-43-9
反应条件
triethylamine; copper(l) chloride in dichloromethane T=20°C; 0.166667 h; Schlenk technique;
参考文献
Xu, Jian; Zhang, Pengbo; Gao, Yuzhen; Chen, Yiyin; Tang, Guo; Zhao, Yufen
Journal of Organic Chemistry, 2013 , vol. 78, # 16 p. 8176 - 8183
612-62-4
2-氯喹啉
+
4559-70-0
二苯基磷氧
→
反应条件
91239-45-1
反应条件
NiCl2((PPh3)P)2; potassium carbonate in N,N-dimethyl-formamide T=50°C; Inert atmosphere;
参考文献
Zhang, Hong-Yu; Sun, Meng; Ma, Yan-Na; Tian, Qiu-Ping; Yang, Shang-Dong
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 48 p. 9627 - 9633
59-31-4
2-羟基喹啉
+
4559-70-0
二苯基磷氧
→
反应条件
91239-45-1
反应条件
1: 2-hydroxyquinoline With potassium carbonate; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate in acetonitrile T=100°C; 3 h; Inert atmosphere; 2: diphenylphosphine oxide With [1,3-bis(diphenylphosphino) propane] dichloronickel(II) in acetonitrile T=100°C; 18 h; Inert atmosphere;
参考文献
Zhao, Yu-Long; Wu, Guo-Jie; Han, Fu-She
Chemical Communications, 2012 , vol. 48, # 47 p. 5868 - 5870
586-76-5
4-溴苯甲酸
+
4559-70-0
二苯基磷氧
→
反应条件
2272-04-0
反应条件
palladium 10 on activated carbon; potassium carbonate in water T=180°C; 1 h; Microwave irradiation;
参考文献
Paul Scherrer Institut; Ranocchiari, Marco; Rummelt, Stephan; Van Bokhoven, Jeroen A.
Patent: EP2626362 A1, 2013 ;
Location in patent: Page/Page column 5 ;
619-58-9
+
4559-70-0
二苯基磷氧
→
反应条件
2272-04-0
反应条件
palladium on activated charcoal; potassium carbonate in water T=100°C; 1 h; Green chemistry; Catalytic behavior; Reagent/catalystTemperature;
参考文献
Paul Scherrer Institut; Ranocchiari, Marco; Rummelt, Stephan; Van Bokhoven, Jeroen A.
Patent: EP2626362 A1, 2013 ;
Location in patent: Paragraph 0009; 0010 ;
4559-70-0
二苯基磷氧
+
74-11-3
→
反应条件
2272-04-0
反应条件
palladium 10 on activated carbon; potassium carbonate in water T=180°C; 1 h; Microwave irradiation;
参考文献
Rummelt, Stephan M.; Ranocchiari, Marco; Van Bokhoven, Jeroen A.
Organic Letters, 2012 , vol. 14, # 8 p. 2188 - 2190
109-65-9
+
4559-70-0
二苯基磷氧
→
反应条件
4233-13-0
反应条件
potassium hydroxide; tetra-(n-butyl)ammonium iodide in benzene T=80°C; 2 h;
参考文献
Tsvetkov, E. N.; Bondarenko, N. A.; Malakhova, I. G.; Kabachnik, M. I.
J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 1 p. 11 - 26,8 - 22
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