4-硝基重氮苯四氟硼酸盐合成路线 (共 247 条)
反应条件
1: NaH2PO4, Na2HPO4 / acetonitrile; H2O / 2 h 2: NaClO4, HClO4 / acetonitrile; H2O / 31.2 °C / other buffer View Scheme
参考文献
Kelly, Richard P.; Penton, John R.; Zollinger, Heinrich
Helvetica Chimica Acta, 1982 , vol. 65, # 1 p. 122 - 132
反应条件
hydrogenchloride in water; acetonitrile 12 h; Ambient temperature; Yield given;
参考文献
Kelly, Richard P.; Penton, John R.; Zollinger, Heinrich
Helvetica Chimica Acta, 1982 , vol. 65, # 1 p. 122 - 132
反应条件
triethyl amine hydrochloride in acetonitrile effect of reagent concentration, solvent; Rate constantProduct distribution;
参考文献
Stovpovoi, P. A.; Bagal, I. L.; El'tsov, A. V.
J. Gen. Chem. USSR (Engl. Transl.), 1986 , vol. 56, # 8 p. 1859 - 1872,1642 - 1654
反应条件
sodium hydroxide T=20°C;
参考文献
Bagal; Luchkevich; El'tsov
Russian Journal of General Chemistry, 1996 , vol. 66, # 1 p. 119 - 132
反应条件
palladium diacetate; SIDip*HCl in 1,4-dioxane T=100°C; P=760 Torr; 5 h;
参考文献
Andrus, Merritt B.; Ma, Yudao; Zang, Yunfu; Song, Chun
Tetrahedron Letters, 2002 , vol. 43, # 50 p. 9137 - 9140
反应条件
agarose hydrogel-supported palladium nanoparticles in methanol; water T=20°C; Suzuki-Miyaura Coupling; 10 h; Green chemistry;
参考文献
Gholinejad, Mohammad
Applied Organometallic Chemistry, 2013 , vol. 27, # 1 p. 19 - 22
参考文献
Hecht; El-Bayoumy; Tulley; LaVoie
Journal of Medicinal Chemistry, 1979 , vol. 22, # 8 p. 981 - 987
反应条件
copper; magnesium sulfate in acetone; benzene
参考文献
Cadogan,J.I.G. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1972 , p. 2555 - 2562
反应条件
(3aS,7aS)-1,3-di-o-tolyl-octahydro-benzoimidazole-2-thione; palladium diacetate in tetrahydrofuran T=20°C; Suzuki reaction; 10 h;
参考文献
Advanced Synthesis and Catalysis, , vol. 346, # 13-15 p. 1669 - 1673
反应条件
palladium diacetate; SIDip*HCl in 1,4-dioxane T=100°C; P=760 Torr; 5 h;
参考文献
Tetrahedron Letters, , vol. 43, # 50 p. 9137 - 9140