4-硝基重氮苯四氟硼酸盐合成路线 （共 247 条）
反应条件
1: With potassium hydroxide in water T=0 - 20°C; pH=8; 2: With hydrogenchloride in water T=0°C; pH=2; 1 h;
参考文献
Raymo, Francisco M.; Tomasulo, Massimiliano
Patent: US2009/258429 A1, 2009 ;
Location in patent: Page/Page column 2; 8 ;
反应条件
in water 0.166667 h;
参考文献
Bagal, I. L.; Zul'figarov, O. S.; Yurchenko, V. V.; Trachevskii, V. V.; El'tsov, A. V.
J. Gen. Chem. USSR (Engl. Transl.), 1992 , vol. 62, # 4.2. p. 928 - 934,762 - 767
反应条件
N-(4-nitrophenyl)thiobenzamide in acetone T=20°C; 2 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Kandror, I.I.; Bragina, I.O.; Freidlina, R.Kh.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 11 p. 2418 - 2421
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 11 p. 2640 - 2642
反应条件
in acetone T=20°C; 2 h; other thiobenzanilides, other phenyldiazonium tetrafluoroborides; Mechanism;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 33, # 11 p. 2418 - 2421
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 11 p. 2640 - 2642
反应条件
(3aS,7aS)-1,3-di-o-tolyl-octahydro-benzoimidazole-2-thione; palladium diacetate in tetrahydrofuran T=20°C; Suzuki reaction; 10 h;
参考文献
Mingji, Dai; Liang, Bo; Wang, Cuihua; You, Zejin; Xiang, Jing; Dong, Guangbin; Chen, Jiahua; Yang, Zhen
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1669 - 1673
反应条件
palladium diacetate; SIDip*HCl in 1,4-dioxane T=100°C; P=760 Torr; 5 h;
参考文献
Tetrahedron Letters, , vol. 43, # 50 p. 9137 - 9140
反应条件
palladium diacetate in diethyl ether; acetonitrile 1 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Kikukawa, Kiyoshi; Idemoto, Tohru; Katayama, Atsuhiko; Kono, Kiyoshi; Wada, Fumio; Matsuda, Tsutomu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1511 - 1514
反应条件
palladium diacetate 1 h; Ambient temperaturedifferent solvents (MeCN-Et2O, DME, MeCN) without and with additive ( 2,6-di-t-butylphenol); Product distribution;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1511 - 1514
反应条件
palladium diacetate 1 h; Ambient temperaturedifferent solvents (MeCN-Et2O, DME, MeCN) without and with additive ( 2,6-di-t-butylphenol); Product distribution;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1511 - 1514
反应条件
iron(II) chloride in tetrachloromethane T=60°C; 3 h;
参考文献
Ding, Yiyuan; Song, Qingbao; Cheng, Kai; Qi, Chenze
Tetrahedron Letters, 2012 , vol. 53, # 46 p. 6269 - 6272,4
