4-硝基重氮苯四氟硼酸盐合成路线 (共 247 条)
反应条件
copper trifluoromethanesulfonate in acetonitrile T=0 - 20°C; 22 h;
参考文献
Tetrahedron, , vol. 63, # 25 p. 5614 - 5621
反应条件
in N,N-dimethyl-formamide T=60°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Markgraf, J. Hodge; Chang, Raymond; Cort, John R.; Durant Jr., Joseph L.; Finkelstein, Manuel; Gross, Andrew W.; Lavyne, Michael H.; Moore, W. Michael; Petersen, Raymond C.; Ross, Sidney D.
Tetrahedron, 1997 , vol. 53, # 29 p. 10009 - 10018
反应条件
hydrogenchloride in water T=50°C; KineticsProduct distribution; Further Variations:acidity, solvent composition;
参考文献
Pazo-Llorente, Roman; Maskill, Howard; Bravo-Diaz, Carlos; Gonzalez-Romero, Elisa
European Journal of Organic Chemistry, 2006 , # 9 p. 2201 - 2209
反应条件
azamacrocyclic palladium(0) in 1,4-dioxane T=20°C; Suzuki-Miyaura cross-coupling; 3 h;
参考文献
European Journal of Organic Chemistry, , # 1 p. 158 - 166
反应条件
in acetonitrile Ambient temperature;
参考文献
Journal of Organometallic Chemistry, , vol. 270, # 3 p. 277 - 282
反应条件
tetrakis(triphenylphosphine) palladium(0); tetra-(n-butyl)ammonium iodide; potassium carbonate in acetonitrile T=60°C; Inert atmosphereDarkness;
参考文献
Cacchi, Sandro; Fabrizi, Giancarlo; Goggiamani, Antonella; Perboni, Alcide; Sferrazza, Alessio; Stabile, Paolo
Organic Letters, 2010 , vol. 12, # 14 p. 3279 - 3281
反应条件
potassium phosphate; copper(l) iodide; 1,10-phenanthroline; tetra-(n-butyl)ammonium iodide in dimethyl sulfoxide; acetonitrile T=130°C; 4 h; Inert atmosphereSchlenk technique;
参考文献
Zhu, Xingyi; Li, Feng; Su, Weike
Tetrahedron Letters, 2013 , vol. 54, # 10 p. 1285 - 1289
反应条件
tetrakis(triphenylphosphine) palladium(0) in ethylene glycol dimethyl ether T=20°C;
参考文献
Frohn, Hermann-Josef; Adonin, Nicolay Yu.; Bardin, Vadim V.; Starichenko, Vladimir F.
Journal of Fluorine Chemistry, 2002 , vol. 117, # 2 p. 115 - 120
反应条件
in water 0.0333333 h; pH 9.0;
参考文献
Bagal, I. L.; Zul'figarov, O. S.; Yurchenko, V. V.; Trachevskii, V. V.; El'tsov, A. V.
J. Gen. Chem. USSR (Engl. Transl.), 1992 , vol. 62, # 4.2. p. 928 - 934,762 - 767
反应条件
in water 0.166667 h;
参考文献
Bagal, I. L.; Zul'figarov, O. S.; Yurchenko, V. V.; Trachevskii, V. V.; El'tsov, A. V.
J. Gen. Chem. USSR (Engl. Transl.), 1992 , vol. 62, # 4.2. p. 928 - 934,762 - 767