4-硝基重氮苯四氟硼酸盐合成路线 （共 247 条）
反应条件
Cu(BF4)2 in water; acetone T=-10 - -5°C;
参考文献
Gorbovoi; Baranovskii; Koval'skii; Grishchuk
Russian Journal of General Chemistry, 2002 , vol. 72, # 8 p. 1230 - 1232
反应条件
Na[B(3,5-(CF3)2C6H3)4] in dichloromethane 2 h; Ambient temperature;
参考文献
Iwamoto, Hidetoshi; Yoshimura, Masaji; Sonoda, Takaaki; Kobayashi, Hiroshi
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 3 p. 796 - 801
反应条件
magnesium 1.) THF, reflux, 2.) THF, 30 deg C, 35 s; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Singh, P. R.; Khanna, R. K.; Jayaraman, B.
Tetrahedron Letters, 1982 , vol. 23, # 51 p. 5475 - 5478
反应条件
5 Pd/BaCO3 in methanol T=25°C; 12 h;
参考文献
Felpin, Francois-Xavier; Fouquet, Eric
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 6 p. 863 - 868
反应条件
palladium diacetate; SIDip*HCl in 1,4-dioxane T=100°C; P=760 Torr; 5 h;
参考文献
Tetrahedron Letters, , vol. 43, # 50 p. 9137 - 9140
反应条件
1 Pd/C in methanol T=50°C; Suzuki-Miyaura reaction; 0.0833333 h; Inert atmosphere;
参考文献
Bonin, Helene; Delbrayelle, Dominique; Demonchaux, Patrice; Gras, Emmanuel
Chemical Communications, 2010 , vol. 46, # 15 p. 2677 - 2679
反应条件
copper(l) iodide; palladium diacetate in isopropyl alcohol T=25°C; Suzuki-Miyaura reaction; 48 h; Inert atmosphere;
参考文献
Chemical Communications, , vol. 46, # 15 p. 2677 - 2679
反应条件
in N,N-dimethyl-formamide T=60°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Markgraf, J. Hodge; Chang, Raymond; Cort, John R.; Durant Jr., Joseph L.; Finkelstein, Manuel; Gross, Andrew W.; Lavyne, Michael H.; Moore, W. Michael; Petersen, Raymond C.; Ross, Sidney D.
Tetrahedron, 1997 , vol. 53, # 29 p. 10009 - 10018
反应条件
in acetonitrile T=2°C; Photolysis; Product distribution;
参考文献
Slegt, Micha; Overkleeft, Hermen S.; Lodder, Gerrit
European Journal of Organic Chemistry, 2007 , # 32 p. 5364 - 5375
反应条件
2: H2 / Pd-C / ethanol View Scheme
参考文献
Hecht; El-Bayoumy; Tulley; LaVoie
Journal of Medicinal Chemistry, 1979 , vol. 22, # 8 p. 981 - 987
