4-硝基重氮苯四氟硼酸盐合成路线 (共 247 条)
反应条件
copper in dichloromethane 64 h;
参考文献
Lorris, Maria E.; Abramovitch, Rudolph A.; Marquet, Jorge; Moreno-Manas, Marcial
Tetrahedron, 1992 , vol. 48, # 33 p. 6909 - 6916
反应条件
copper(l) iodide; palladium diacetate in isopropyl alcohol T=25°C; Suzuki-Miyaura reaction; 48 h; Inert atmosphere;
参考文献
Chemical Communications, , vol. 46, # 15 p. 2677 - 2679
反应条件
magnesium 1.) THF, reflux, 2.) THF, 30 deg C, 90 s; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Singh, P. R.; Khanna, R. K.; Jayaraman, B.
Tetrahedron Letters, 1982 , vol. 23, # 51 p. 5475 - 5478
反应条件
sodium acetate; palladium diacetate in acetonitrile P=6619.6 Torr; 1 h; Ambient temperature;
参考文献
Nagira, Kazuhiko; Kikukawa, Kiyoshi; Wada, Fumio; Matsuda, Tsutomu
Journal of Organic Chemistry, 1980 , vol. 45, # 12 p. 2365 - 2368
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetra-(n-butyl)ammonium iodide; diethylamine in acetonitrile
T=20°C; Sonogashira coupling; 1.5 h; Inert atmosphere;
参考文献
Fabrizi, Giancarlo; Goggiamani, Antonella; Sferrazza, Alessio; Cacchi, Sandro
Angewandte Chemie - International Edition, 2010 , vol. 49, # 24 p. 4067 - 4070
反应条件
palladium diacetate in diethyl ether; acetonitrile
2.3 h; Ambient temperature; Yield given;
参考文献
Kikukawa, Kiyoshi; Idemoto, Tohru; Katayama, Atsuhiko; Kono, Kiyoshi; Wada, Fumio; Matsuda, Tsutomu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1511 - 1514
参考文献
Bronberger, Franz; Huisgen, Rolf
Tetrahedron Letters, 1984 , vol. 25, # 1 p. 65 - 68
反应条件
palladium diacetate in ethanol; water
T=20°C; Heck arylation; 0.5 h;
参考文献
Artuso, Emma; Barbero, Margherita; Degani, Iacopo; Dughera, Stefano; Fochi, Rita
Tetrahedron, 2006 , vol. 62, # 13 p. 3146 - 3157
反应条件
2-iodo-propane; copper in dimethyl sulfoxide
3 h; Ambient temperature; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Citterio, Attilio; Vismara, Elena; Bernardi, Rosanna
Journal of Chemical Research, Miniprint, 1983 , # 4 p. 876 - 890
反应条件
copper in dimethyl sulfoxide
T=20°C; 1 h; other catalyst, other time; Rate constantMechanismProduct distribution;
参考文献
Citterio, Attilio; Vismara, Elena; Bernardi, Rosanna
Journal of Chemical Research, Miniprint, 1983 , # 4 p. 876 - 890