4-硝基重氮苯四氟硼酸盐合成路线 (共 247 条)
反应条件
trimethylsilylazide in N,N-dimethyl-formamide
1 h; Ambient temperature;
参考文献
Keumi, Takashi; Umeda, Toshiaki; Inoue, Yoshinori; Kitajima, Hidehiko
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 1 p. 89 - 95
反应条件
sodium acetate in water; acetic acid
T=0°C; 1.5 h;
参考文献
Zlotin, S. G.; Prokshits, O. V.; Luk'yanov, O. A.
Bull. Russ. Acad. Sci. Div. Chem. Sci. (Engl. Transl.), 1992 , vol. 41, # 8.2 p. 1911 - 1913,1495 - 1496
反应条件
1,10-phenanthroline; Cu(BF4)2; [Cu(CH3CN)4]BF4 in acetonitrile
T=0 - 5°C;
参考文献
Beletskaya, Irina P.; Sigeev, Alexander S.; Peregudov, Alexander S.; Petrovskii, Pavel V.
Mendeleev Communications, 2006 , # 5 p. 250 - 251
反应条件
bis(dibenzylideneacetone)-palladium(0) in acetonitrile
T=25°C; Yield given. Yields of byproduct given;
参考文献
Kikukawa, Kiyoshi; Ikenaga, Kazutoshi; Wada, Fumio; Matsuda, Tsutomu
Chemistry Letters, 1983 , p. 1337 - 1340
反应条件
bis(dibenzylideneacetone)-palladium(0) in acetonitrile
T=25°C; Yield given. Yields of byproduct given;
参考文献
Kikukawa, Kiyoshi; Ikenaga, Kazutoshi; Wada, Fumio; Matsuda, Tsutomu
Chemistry Letters, 1983 , p. 1337 - 1340
反应条件
palladium diacetate; SIDip*HCl in 1,4-dioxane
T=100°C; P=760 Torr; 5 h;
参考文献
Andrus, Merritt B.; Ma, Yudao; Zang, Yunfu; Song, Chun
Tetrahedron Letters, 2002 , vol. 43, # 50 p. 9137 - 9140
反应条件
aluminium hydroxide-supported palladium nanoparticles in methanol
T=0°C; Suzuki-Miyaura cross-coupling; 12 h;
参考文献
Li, Xing; Yan, Xu-Ying; Chang, Hong-Hong; Wang, Li-Chao; Zhang, Yan; Chen, Wen-Wen; Li, Yan-Wei; Wei, Wen-Long
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 3 p. 495 - 497
反应条件
palladium 10 on activated carbon in methanol
Suzuki-Miyaura cross-coupling; RefluxUnder air;
参考文献
Hanna Jr., James M.; Varnedoe, Lee S.; Angel, Brad D.; McClellan, Joshua L.
Letters in Organic Chemistry, 2010 , vol. 7, # 1 p. 1 - 6
反应条件
C33H25BF2I2N2 in dimethyl sulfoxide
T=20°C; 1 h; Inert atmosphereIrradiation; Catalytic behavior; Reagent/catalyst;
参考文献
Huang, Ling; Zhao, Jianzhang
RSC Advances, 2013 , vol. 3, # 45 p. 23377 - 23388
反应条件
in dimethyl sulfoxide
参考文献
Russell,G.A. et al.
Journal of the American Chemical Society, 1971 , vol. 93, p. 5839 - 5845