4-硝基重氮苯四氟硼酸盐合成路线 (共 247 条)
参考文献
Kazankov, M. V.; Makshanova, N. P.; Sadovykh, E. G.
Russian Journal of Organic Chemistry, 1995 , vol. 31, # 3 p. 414 - 417
Zhurnal Organicheskoi Khimii, 1995 , vol. 31, # 3 p. 453 - 457
反应条件
boron trifluoride diethyl etherate T=120 - 125°C; 1 h;
参考文献
Shinhama; Aki; Furuta; Minamikawa
Synthetic Communications, 1993 , vol. 23, # 11 p. 1577 - 1582
反应条件
N-(4-nitrophenyl)thiobenzamide in acetone T=20°C; 2 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Kandror, I.I.; Bragina, I.O.; Freidlina, R.Kh.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 11 p. 2418 - 2421
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 11 p. 2640 - 2642
反应条件
in acetone T=20°C; 2 h; other thiobenzanilides, other phenyldiazonium tetrafluoroborides; Mechanism;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 33, # 11 p. 2418 - 2421
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 11 p. 2640 - 2642
反应条件
dibenzo-18-crown-6; potassium bromide; copper(ll) bromide; 1,10-phenanthroline; copper(I) bromide in acetonitrile T=20°C; Sandmeyer bromination; 0.333333 h;
参考文献
Beletskaya, Irina P.; Sigeev, Alexander S.; Peregudov, Alexander S.; Petrovskii, Pavel V.
Synthesis, 2007 , # 16 p. 2534 - 2538
反应条件
T=75°C; Geschwindigkeit der Reaktion;
参考文献
Lewis; Hinds
Journal of the American Chemical Society, 1952 , vol. 74, p. 304,306
反应条件
T=75°C; Geschwindigkeit der Reaktion;
参考文献
Lewis; Hinds
Journal of the American Chemical Society, 1952 , vol. 74, p. 304,306
反应条件
1 Pd/C in methanol T=50°C; Suzuki-Miyaura reaction; 0.5 h; Inert atmosphere;
参考文献
Bonin, Helene; Delbrayelle, Dominique; Demonchaux, Patrice; Gras, Emmanuel
Chemical Communications, 2010 , vol. 46, # 15 p. 2677 - 2679
反应条件
sodium acetate in water; acetic acid T=0°C; 1.5 h;
参考文献
Bull. Russ. Acad. Sci. Div. Chem. Sci. (Engl. Transl.), , vol. 41, # 8.2 p. 1911 - 1913,1495 - 1496
反应条件
N-(4-nitrophenyl)thiobenzamide in acetone T=20°C; 2 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Kandror, I.I.; Bragina, I.O.; Freidlina, R.Kh.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 11 p. 2418 - 2421
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 11 p. 2640 - 2642