4-硝基重氮苯四氟硼酸盐合成路线 （共 247 条）
反应条件
in methanol
T=0°C; 0.5 h;
参考文献
Khanna, Rajive K.; Jiang, Yong M.; Singh
Tetrahedron Letters, 1991 , vol. 32, # 40 p. 5449 - 5452
反应条件
in Loesung vom pH 6;
参考文献
Huenig; Boes
Justus Liebigs Annalen der Chemie, 1953 , vol. 579, p. 28,42, 43
反应条件
2: (reduction)
View Scheme
参考文献
Hecht; El-Bayoumy; Tulley; LaVoie
Journal of Medicinal Chemistry, 1979 , vol. 22, # 8 p. 981 - 987
反应条件
2: (reduction)
3: Ag2CO3 / CH2Cl2
View Scheme
参考文献
Hecht; El-Bayoumy; Tulley; LaVoie
Journal of Medicinal Chemistry, 1979 , vol. 22, # 8 p. 981 - 987
参考文献
Markgraf, J. Hodge; Chang, Raymond; Cort, John R.; Durant Jr., Joseph L.; Finkelstein, Manuel; Gross, Andrew W.; Lavyne, Michael H.; Moore, W. Michael; Petersen, Raymond C.; Ross, Sidney D.
Tetrahedron, 1997 , vol. 53, # 29 p. 10009 - 10018
反应条件
Ambient temperature; Yield given;
参考文献
Kaupp, Gerd; Herrmann, Andreas
Advanced Synthesis and Catalysis, 1997 , vol. 339, # 3 p. 256 - 260
反应条件
sodium acetate in ethanol
T=0 - 5°C; 4 h;
参考文献
Matiychuk, Vasyl S.; Potopnyk, Mykhaylo A.; Obushak, Mykola D.
Journal of Heterocyclic Chemistry, 2013 , vol. 50, # SUPPL.1 p. E43-E47
反应条件
water; sodium acetate in acetonitrile
T=0°C; 1.16667 h; Inert atmosphere; Reagent/catalystSolvent;
参考文献
Basavanag, Unnamatla M. V.; Dos Santos, Aurelie; El Kaim, Laurent; Gamez-Montano, Rocio; Grimaud, Laurence
Angewandte Chemie - International Edition, 2013 , vol. 52, # 28 p. 7194 - 7197
Angew. Chem., 2013 , vol. 125, # 28 p. 7335 - 7338,4
反应条件
1: 41.4 percent / acetonitrile / 12 h / Ambient temperature
2: 60 percent / potassium phenoxide / acetonitrile / 4 h / Heating
3: 1.) potassium hydroxide, 2.) copper / 1.) 100 deg C, 3h, 2.) 200 deg C, 12h
View Scheme
参考文献
Abramovitch, Rudolph A.; Inbasekaran, Muthiah N.; Kato, Shozo; Radzikowska, Teresa A.; Tomasik, Piotr
Journal of Organic Chemistry, 1983 , vol. 48, # 5 p. 690 - 695
参考文献
Huenig; Boes
Justus Liebigs Annalen der Chemie, 1953 , vol. 579, p. 28,42, 43
