4-硝基重氮苯四氟硼酸盐合成路线 （共 247 条）
反应条件
C33H25BF2I2N2 in dimethyl sulfoxide
T=20°C; 1 h; Inert atmosphereIrradiation; Catalytic behavior; Reagent/catalyst;
参考文献
Huang, Ling; Zhao, Jianzhang
RSC Advances, 2013 , vol. 3, # 45 p. 23377 - 23388
反应条件
1: iodobenzene / dimethylformamide / 0.67 h / 60 °C
2: dimethylformamide / 60 °C
View Scheme
参考文献
Markgraf, J. Hodge; Chang, Raymond; Cort, John R.; Durant Jr., Joseph L.; Finkelstein, Manuel; Gross, Andrew W.; Lavyne, Michael H.; Moore, W. Michael; Petersen, Raymond C.; Ross, Sidney D.
Tetrahedron, 1997 , vol. 53, # 29 p. 10009 - 10018
反应条件
in N,N-dimethyl-formamide
T=60°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Markgraf, J. Hodge; Chang, Raymond; Cort, John R.; Durant Jr., Joseph L.; Finkelstein, Manuel; Gross, Andrew W.; Lavyne, Michael H.; Moore, W. Michael; Petersen, Raymond C.; Ross, Sidney D.
Tetrahedron, 1997 , vol. 53, # 29 p. 10009 - 10018
反应条件
in ethanol; water
T=20°C; 1 h;
参考文献
Jackson, Anthony H.; Prasitpan, Noojaree; Shannon, Patrick V. R.; Tinker, Alan C.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 2543 - 2552
反应条件
1: 94 percent / ethanol; H2O
2: 89 percent / potassium carbonate / acetone / 2 h / 30 - 35 °C
View Scheme
参考文献
Jackson, Anthony H.; Prasitpan, Noojaree; Shannon, Patrick V. R.; Tinker, Alan C.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 2543 - 2552
反应条件
in ethanol; water
0.333333 h;
参考文献
Jackson, Anthony H.; Lynch, Patrick P.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1987 , p. 1483 - 1488
反应条件
in acetonitrile
T=20°C; 0.0333333 h;
参考文献
Jackson, Anthony H.; Prasitpan, Noojaree; Shannon, Patrick V. R.; Tinker, Alan C.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 2543 - 2552
反应条件
1: iodobenzene / dimethylformamide / 0.67 h / 60 °C
2: dimethylformamide / 60 °C
View Scheme
参考文献
Markgraf, J. Hodge; Chang, Raymond; Cort, John R.; Durant Jr., Joseph L.; Finkelstein, Manuel; Gross, Andrew W.; Lavyne, Michael H.; Moore, W. Michael; Petersen, Raymond C.; Ross, Sidney D.
Tetrahedron, 1997 , vol. 53, # 29 p. 10009 - 10018
反应条件
in N,N-dimethyl-formamide
T=60°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Markgraf, J. Hodge; Chang, Raymond; Cort, John R.; Durant Jr., Joseph L.; Finkelstein, Manuel; Gross, Andrew W.; Lavyne, Michael H.; Moore, W. Michael; Petersen, Raymond C.; Ross, Sidney D.
Tetrahedron, 1997 , vol. 53, # 29 p. 10009 - 10018
反应条件
1: 55 percent / tetrahydrothiophene 1,1-dioxide / 2 h / 80 °C
2: 5 h / 180 °C
View Scheme
参考文献
Abramovitch, Rudolph A.; Alvernhe, Gerard; Bartnik, Romuald; Dassanayake, Nissanke L.; Inbasekaran, Mutiah N.; Kato, Shiego
Journal of the American Chemical Society, 1981 , vol. 103, # 15 p. 4558 - 4565
