4-硝基重氮苯四氟硼酸盐合成路线 (共 247 条)
反应条件
in acetonitrile T=50°C; Arylation; Trifluoromethylthiodediazoniation;
参考文献
Adams, Dave J.; Goddard, Andrew; Clark, James H.; Macquarrie, Duncan J.
Chemical Communications, 2000 , # 11 p. 987 - 988
反应条件
aluminium hydroxide-supported palladium nanoparticles in methanol T=20°C; Suzuki-Miyaura cross-coupling; 6 h;
参考文献
Li, Xing; Yan, Xu-Ying; Chang, Hong-Hong; Wang, Li-Chao; Zhang, Yan; Chen, Wen-Wen; Li, Yan-Wei; Wei, Wen-Long
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 3 p. 495 - 497
反应条件
1 Pd/C in methanol T=50°C; Suzuki-Miyaura reaction; 0.166667 h; Inert atmosphere;
参考文献
Bonin, Helene; Delbrayelle, Dominique; Demonchaux, Patrice; Gras, Emmanuel
Chemical Communications, 2010 , vol. 46, # 15 p. 2677 - 2679
反应条件
palladium diacetate; SIDip*HCl in 1,4-dioxane T=100°C; P=760 Torr; 5 h;
参考文献
Tetrahedron Letters, , vol. 43, # 50 p. 9137 - 9140
反应条件
cesium fluoride; Na2[PdCl4] in methanol T=40°C; Arylation; cross-coupling; 24 h;
参考文献
Willis; Strongin
Tetrahedron Letters, 2000 , vol. 41, # 33 p. 6271 - 6274
反应条件
xanthone powder in acetonitrile Irradiation;
参考文献
Milanesi, Silvia; Fagnoni, Maurizio; Albini, Angelo
Chemical Communications, 2003 , # 2 p. 216 - 217
反应条件
in acetonitrile T=20°C; Photolysis;
参考文献
Journal of Organic Chemistry, , vol. 70, # 2 p. 603 - 610
反应条件
SIDip*HCl; palladium diacetate in tetrahydrofuran T=20°C; 1 h;
参考文献
Ma, Yudao; Song, Chun; Jiang, Wei; Xue, Guoping; Cannon, John F.; Wang, Xiaomei; Andrus, Merritt B.
Organic Letters, 2003 , vol. 5, # 24 p. 4635 - 4638
反应条件
1: tBuCH2CH2B(H)NiPr2; 4-Nitrobenzenediazonium tetrafluoroborate With biscyclopentadienyliron(II) in acetonitrile T=20°C; 2.5 h; 2: With methanol in acetonitrile T=0 - 20°C; 1 h; 3: 2,3-dimethylbutane-2,3-diol in diethyl ether; acetonitrile T=20°C; 4 h; Reagent/catalyst;
参考文献
UNIVERSITE DE BORDEAUX 1; CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE; PUCHEAULT, Mathieu Jonathan Damien; MARCIASINI, Ludovic Daniel Alain; VAULTIER, Michel
Patent: WO2014/9169 A1, 2014 ;
Location in patent: Page/Page column 56-57 ;
反应条件
diethylenetriamine-N,N,N',N'',N''-pentaacetic acid in phosphate buffer T=37°C; pH=7.2; 0.75 h; Kinetics; Further Variations:Reagents;
参考文献
Quintero; Cabeza; Martinez; Gutierrez
Canadian Journal of Chemistry, 2003 , vol. 81, # 7 p. 832 - 839