4-硝基重氮苯四氟硼酸盐合成路线 （共 247 条）
反应条件
triethylsilane; palladium diacetate in diethyl ether; acetonitrile P=7355.08 Torr; 0.166667 h;
参考文献
Kikukawa, Kiyoshi; Totoki, Takatoshi; Wada, Fumio; Matsuda, Tsutomu
Journal of Organometallic Chemistry, 1984 , vol. 270, # 3 p. 283 - 288
反应条件
palladium diacetate; acetic acid in N,N-dimethyl-formamide T=0 - 5°C; diazonium Heck coupling; 0.45 h; segmented microflow;
参考文献
Ahmed-Omer, Batoul; Barrow, David A.; Wirth, Thomas
Tetrahedron Letters, 2009 , vol. 50, # 26 p. 3352 - 3355
反应条件
Na[B(3,5-(CF3)2C6H3)4] in dichloromethane; water 48 h; Ambient temperature;
参考文献
Iwamoto, Hidetoshi; Yoshimura, Masaji; Sonoda, Takaaki; Kobayashi, Hiroshi
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 3 p. 796 - 801
反应条件
in acetonitrile 7 h; Ambient temperature;
参考文献
Neumann, Wilhelm P.; Wicenec, Christian
Chemische Berichte, 1991 , vol. 124, # 10 p. 2297 - 2301
反应条件
in nitromethane inert atm. 5 h, evapd. in vac., dissolved in CH2Cl2, PPNCl added, extraction with hexane; adsorption chromy., Cr complex not isolated - detected by IR;
参考文献
Legzdins, Peter.; Richter-Addo, Georg B.; Wassink, Berend; Einstein, Frederick W. B.; Jones, Richard H.; Willis, Anthony C.
Journal of the American Chemical Society, 1989 , vol. 111, # 6 p. 2097 - 2104
反应条件
Na[B(3,5-(CF3)2C6H3)4] in dichloromethane; water 12 h; Ambient temperature;
参考文献
Iwamoto, Hidetoshi; Yoshimura, Masaji; Sonoda, Takaaki; Kobayashi, Hiroshi
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 3 p. 796 - 801
反应条件
N,N,N',N,-tetramethylethylenediamine; potassium chloride; N-benzyl-N,N,N-triethylammonium chloride; copper(l) chloride; copper dichloride in acetonitrile T=20°C; Sandmeyer Reaction; 1 h;
参考文献
Sigeev, A. S.; Beletskaya, I. P.; Petrovskii, P. V.; Peregudov, A. S.
Russian Journal of Organic Chemistry, 2012 , vol. 48, # 8 p. 1055 - 1058,4
Zhurnal Organicheskoi Khimii, 2012 , vol. 48, # 8 p. 1059 - 1062,4
反应条件
sodium chloride; copper dichloride in water; acetone T=0 - 15°C;
参考文献
Grishchuk, B. D.; Gorbovoi, P. M.; Ganushchak, N. I.; Brush, D. M.; Kudrik, E. Ya.
Russian Journal of General Chemistry, 1993 , vol. 63, # 7.2 p. 1156 - 1158
Zhurnal Obshchei Khimii, 1993 , vol. 63, # 7 p. 1655 - 1658
反应条件
hydrogenchloride T=60°C; dediazoniation; 22 h; Product distributionKinetics;
参考文献
International Journal of Chemical Kinetics, , vol. 32, # 7 p. 419 - 430
反应条件
Cu(BF4)2 in water; acetone addn. of NO2C6H4N2BF4 to 1,4-bis(acryloyloxy)butane, Cu(BF4)2 and NaSCN in aq. acetone (1:2) for 45-60 min; cooling at -10 - -5°C for 2 h; evolution of N2, treatment of residual with Et2O, extn., washing with water, drying with MgSO4, removal of ether, chromy.;
参考文献
Russian Journal of General Chemistry, , vol. 72, # 8 p. 1230 - 1232
