1: 34 percent / lithium aluminium hydride / diethyl ether; dibutyl ether / 4 h / Heating 2: tert-butyl hyponitrite, triethylamine / dimethyl ether / 1 h / -78 °C 3: hexane / -10 °C / other solvents, temperatures; Ea, log A, ΔH<*>, ΔS<*>, ET, ΔG<*> View Scheme

1: 34 percent / lithium aluminium hydride / diethyl ether; dibutyl ether / 4 h / Heating 2: tert-butyl hyponitrite, triethylamine / dimethyl ether / 1 h / -78 °C 3: hexane / -10 °C / other solvents, temperatures; Ea, log A, ΔH<*>, ΔS<*>, ET, ΔG<*> View Scheme

1: 34 percent / lithium aluminium hydride / diethyl ether; dibutyl ether / 4 h / Heating 2: tert-butyl hyponitrite, triethylamine / dimethyl ether / 1 h / -78 °C 3: hexane / -10 °C / other solvents, temperatures; Ea, log A, ΔH<*>, ΔS<*>, ET, ΔG<*> View Scheme