反应条件
1.1: potassium hexamethyldisilylazide / 1,2-dimethoxy-ethane / 1 h / -78 °C 1.2: 1,2-dimethoxy-ethane / -78 - 20 °C 2.1: CAN; H2O / acetone 3.1: aq. NaOH / tetrahydrofuran; methanol 4.1: 61 percent / MsCl; Et3N; 2,4,6-trichlorobenzoyl chloride / 4-DMAP / toluene / Heating 5.1: 77 percent / TBAF / tetrahydrofuran / 20 °C View Scheme
参考文献
Trost, Barry M.; Crawley, Matthew L.
Journal of the American Chemical Society, 2002 , vol. 124, # 32 p. 9328 - 9329
