反应条件
1.1: LiAlH(OCMe3)3 / tetrahydrofuran / -78 °C 2.1: O3 / CH2Cl2 / -78 °C 3.1: 34 percent / scandium triflate / acetonitrile / -20 - 0 °C 4.1: 53 percent / n-BuLi / tetrahydrofuran / -20 - 0 °C 5.1: potassium hexamethyldisilazane / tetrahydrofuran / -78 °C 5.2: PhSeCl / -23 °C 5.3: 31 percent / H2O2 / acetic acid View Scheme
参考文献
Wu, Baogen; Karle, Jean M.; Watkins, E. Blake; Avery, Mitchell A.
Tetrahedron Letters, 2002 , vol. 43, # 22 p. 4095 - 4098