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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
457644-50-7
合成路线
（共 11 条）
457644-50-7
→
反应条件
19384-00-0
2-薁并l
反应条件
water; dihydrogen peroxide in ethanol T=20°C; 2 h;
参考文献
Kurotobi, Kei; Miyauchi, Masato; Takakura, Katsuto; Murafuji, Toshihiro; Sugihara, Yoshikazu
European Journal of Organic Chemistry, 2003 , # 18 p. 3663 - 3665
624-31-7
4-碘甲苯
+
457644-50-7
→
反应条件
111679-38-0
+
275-51-4
奥苷菊环
反应条件
tris(dibenzylideneacetone)dipalladium (0); tri-tert-butyl phosphine; caesium carbonate in 1,4-dioxane T=80°C; Miyaura-Suzuki cross-coupling; 24 h;
参考文献
Ito, Shunji; Terazono, Tomomi; Kubo, Takahiro; Okujima, Tetsuo; Morita, Noboru; Murafuji, Toshihiro; Sugihara, Yoshikazu; Fujimori, Kunihide; Kawakami, Jun; Tajiri, Akio
Tetrahedron, 2004 , vol. 60, # 25 p. 5357 - 5366
615-54-3
1,2,4-三溴苯
+
457644-50-7
→
反应条件
275-51-4
奥苷菊环
反应条件
tris(dibenzylideneacetone)dipalladium (0); tri-tert-butyl phosphine; caesium carbonate in 1,4-dioxane T=80°C; Miyaura-Suzuki cross-coupling; 24 h;
参考文献
Ito, Shunji; Terazono, Tomomi; Kubo, Takahiro; Okujima, Tetsuo; Morita, Noboru; Murafuji, Toshihiro; Sugihara, Yoshikazu; Fujimori, Kunihide; Kawakami, Jun; Tajiri, Akio
Tetrahedron, 2004 , vol. 60, # 25 p. 5357 - 5366
106-43-4
对氯甲苯
+
457644-50-7
→
反应条件
82893-99-0
+
111679-38-0
+
275-51-4
奥苷菊环
反应条件
barium dihydroxide; Cs2C03; tris(dibenzylideneacetone)dipalladium (0); tri-tert-butyl phosphine in 1,4-dioxane T=80°C; 24 h;
参考文献
Ito, Shunji; Terazono, Tomomi; Kubo, Takahiro; Okujima, Tetsuo; Morita, Noboru; Murafuji, Toshihiro; Sugihara, Yoshikazu; Fujimori, Kunihide; Kawakami, Jun; Tajiri, Akio
Tetrahedron, 2004 , vol. 60, # 25 p. 5357 - 5366
106-37-6
对二溴苯
+
457644-50-7
→
反应条件
19227-07-7
2-苯基-薁
+
275-51-4
奥苷菊环
反应条件
tris(dibenzylideneacetone)dipalladium (0); tri-tert-butyl phosphine; caesium carbonate in 1,4-dioxane T=80°C; Miyaura-Suzuki cross-coupling; 24 h;
参考文献
Ito, Shunji; Terazono, Tomomi; Kubo, Takahiro; Okujima, Tetsuo; Morita, Noboru; Murafuji, Toshihiro; Sugihara, Yoshikazu; Fujimori, Kunihide; Kawakami, Jun; Tajiri, Akio
Tetrahedron, 2004 , vol. 60, # 25 p. 5357 - 5366
626-39-1
1,3,5-三溴苯
+
457644-50-7
→
反应条件
275-51-4
奥苷菊环
反应条件
tris(dibenzylideneacetone)dipalladium (0); tri-tert-butyl phosphine; caesium carbonate in 1,4-dioxane T=80°C; Miyaura-Suzuki cross-coupling; 24 h;
参考文献
Ito, Shunji; Terazono, Tomomi; Kubo, Takahiro; Okujima, Tetsuo; Morita, Noboru; Murafuji, Toshihiro; Sugihara, Yoshikazu; Fujimori, Kunihide; Kawakami, Jun; Tajiri, Akio
Tetrahedron, 2004 , vol. 60, # 25 p. 5357 - 5366
457644-50-7
+
583-53-9
1,2-二溴苯
→
反应条件
19227-07-7
2-苯基-薁
+
275-51-4
奥苷菊环
反应条件
tris(dibenzylideneacetone)dipalladium (0); tri-tert-butyl phosphine; caesium carbonate in 1,4-dioxane T=80°C; Miyaura-Suzuki cross-coupling; 24 h;
参考文献
Ito, Shunji; Terazono, Tomomi; Kubo, Takahiro; Okujima, Tetsuo; Morita, Noboru; Murafuji, Toshihiro; Sugihara, Yoshikazu; Fujimori, Kunihide; Kawakami, Jun; Tajiri, Akio
Tetrahedron, 2004 , vol. 60, # 25 p. 5357 - 5366
636-28-2
1,2,4,5-四溴苯
+
457644-50-7
→
反应条件
275-51-4
奥苷菊环
反应条件
tris(dibenzylideneacetone)dipalladium (0); tri-tert-butyl phosphine; caesium carbonate in 1,4-dioxane T=80°C; Miyaura-Suzuki cross-coupling; 24 h;
参考文献
Ito, Shunji; Terazono, Tomomi; Kubo, Takahiro; Okujima, Tetsuo; Morita, Noboru; Murafuji, Toshihiro; Sugihara, Yoshikazu; Fujimori, Kunihide; Kawakami, Jun; Tajiri, Akio
Tetrahedron, 2004 , vol. 60, # 25 p. 5357 - 5366
106-37-6
对二溴苯
+
457644-50-7
→
反应条件
19227-07-7
2-苯基-薁
+
275-51-4
奥苷菊环
反应条件
tris(dibenzylideneacetone)dipalladium (0); tri-tert-butyl phosphine; caesium carbonate in 1,4-dioxane T=80°C; Miyaura-Suzuki cross-coupling; 24 h;
参考文献
Ito, Shunji; Terazono, Tomomi; Kubo, Takahiro; Okujima, Tetsuo; Morita, Noboru; Murafuji, Toshihiro; Sugihara, Yoshikazu; Fujimori, Kunihide; Kawakami, Jun; Tajiri, Akio
Tetrahedron, 2004 , vol. 60, # 25 p. 5357 - 5366
106-38-7
对溴甲苯
+
457644-50-7
→
反应条件
19227-07-7
2-苯基-薁
+
111679-38-0
反应条件
bis-triphenylphosphine-palladium(II) chloride; barium dihydroxide in ethylene glycol dimethyl ether; water T=80°C; Miyaura-Suzuki cross-coupling; 24 h;
参考文献
Ito, Shunji; Terazono, Tomomi; Kubo, Takahiro; Okujima, Tetsuo; Morita, Noboru; Murafuji, Toshihiro; Sugihara, Yoshikazu; Fujimori, Kunihide; Kawakami, Jun; Tajiri, Akio
Tetrahedron, 2004 , vol. 60, # 25 p. 5357 - 5366
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