1,2-二(4-氟苯基)乙烷合成路线 （共 19 条）
反应条件
NiCl2((PPh3)P)2; zinc in tetrahydrofuran
T=20°C; 18 h; Inert atmosphere;
参考文献
Giedyk; Fedosov; Gryko
Chemical Communications, 2014 , vol. 50, # 36 p. 4674 - 4676
参考文献
Aitken, R. Alan; Hodgson, Philip K. G.; Oyewale, Adebayo O.; Morrison, John J.
Chemical Communications, 1997 , # 13 p. 1163 - 1164
反应条件
dipotassium hydrogenphosphate; silver nitrate; zinc in water
T=30°C; 1 h;
参考文献
Bieber, Lothar W.; Storch, Elisabeth C.; Malvestiti, Ivani; Da Silva, Margarete F.
Tetrahedron Letters, 1998 , vol. 39, # 51 p. 9393 - 9396
反应条件
ammonium nitrate; copper(II) nitrate in acetic acid
2 h; Heating;
参考文献
Cherkashin, M. I.; Chauser, M. G.; Shienok, A. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 2 p. 340 - 341
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 2 p. 376 - 377
参考文献
Trahanovsky,W.S. et al.
Journal of the American Chemical Society, 1968 , vol. 90, p. 2839 - 2842
反应条件
water; naphthalenyllithium in tetrahydrofuran; diethyl ether; Petroleum ether
T=-95°C; 0.75 h; Title compound not separated from byproducts;
参考文献
Smith, Keith; Hou, Daunjie
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , p. 185 - 186
反应条件
anhydrous iron chloride in tetrahydrofuran
T=20°C; 0.5 h; Inert atmosphere;
参考文献
Qian, Xin; Kozak, Christopher M.
Synlett, 2011 , # 6 p. 852 - 856
反应条件
hydrogen; palladium on activated charcoal
参考文献
Gascoyne,J.M. et al.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1977 , p. 1051 - 1057
反应条件
1: 86 percent / NaCN / dimethylformamide; dimethylsulfoxide / 65 h / 20 °C / Heating
2: 83 percent / ammonium nitrate, Cu(NO3)2*6H2O / acetic acid / 2 h / Heating
View Scheme
参考文献
Cherkashin, M. I.; Chauser, M. G.; Shienok, A. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 2 p. 340 - 341
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 2 p. 376 - 377
反应条件
magnesium
Yield given. Multistep reaction;
参考文献
Imrie, C.; Modro, T. A.; Rohwer, E. R.; Wagener, C. C. P.
Journal of Organic Chemistry, 1993 , vol. 58, # 21 p. 5643 - 5649
