2,2,6-三甲基-1-氧杂螺[2.5]辛-5-烯合成路线 （共 57 条）
反应条件
sodium in tetrahydrofuran T=65°C; 12 h;
参考文献
Tetrahedron, , vol. 40, # 9 p. 1629 - 1632
反应条件
lithium aluminium tetrahydride; aluminium trichloride in diethyl ether 8 h; Ambient temperature;
参考文献
Synthesis, , # 11 p. 888 - 889
反应条件
potassium tert-butylate in tetrahydrofuran T=66°C; 7.5 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 34, # 7 p. 636 - 638
反应条件
potassium tert-butylate in dimethyl sulfoxide T=27°C; 0.75 h; var. solvents and temp.; Product distribution;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 34, # 7 p. 636 - 638
反应条件
sodium in tetrahydrofuran T=65°C; 12 h;
参考文献
Tetrahedron, , vol. 40, # 9 p. 1629 - 1632
反应条件
lithium aluminium tetrahydride; aluminium trichloride in diethyl ether 8 h; Ambient temperature;
参考文献
Synthesis, , # 11 p. 888 - 889
反应条件
1: With bis(cyclopentadienyl)titanium dichloride; zinc in tetrahydrofuran; acetonitrile 0.5 h; Inert atmosphere; 2: With sodium dihydrogenphosphate; water in tetrahydrofuran; acetonitrile 0.333333 h; Inert atmosphere; regioselective reaction;
参考文献
Fernandez-Mateos; Encinas Madrazo; Herrero Teijon; Rubio Gonzalez
Journal of Organic Chemistry, 2009 , vol. 74, # 10 p. 3913 - 3918
反应条件
lithium; biphenyl in ethylene glycol dimethyl ether 5.5 h;
参考文献
Pasha, M. Afzal; Ravindranath, B.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 11 p. 1149
反应条件
sodium in tetrahydrofuran T=65°C; 12 h;
参考文献
Tetrahedron, , vol. 40, # 9 p. 1629 - 1632
反应条件
Au-TiO2 nanoparticles in 1,2-dichloro-ethane T=80°C; 2 h; regioselective reaction;
参考文献
Raptis, Christos; Stratakis, Manolis; Garcia, Hermenegildo
Angewandte Chemie, International Edition, 2009 , vol. 48, # 17 p. 3133 - 3136
