2,2,6-三甲基-1-氧杂螺[2.5]辛-5-烯合成路线 （共 57 条）
反应条件
perchloric acid in diethyl ether T=25°C; 1 h; Further byproducts given;
参考文献
Gurudutt, K. N.; Pasha, M. A.; Ravindranath, B.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 820 - 823
反应条件
pyridinium p-toluenesulfonate in acetone T=25°C; 1 h;
参考文献
Gurudutt, K. N.; Pasha, M. A.; Ravindranath, B.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 820 - 823
反应条件
perchloric acid in diethyl ether T=25°C; 1 h; further solvents: acetone, benzene; further acid catalysts: PTS, BF3, Dowex H+, ZnBr2, AlCl3; Product distribution;
参考文献
Gurudutt, K. N.; Pasha, M. A.; Ravindranath, B.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 820 - 823
反应条件
sodium in tetrahydrofuran T=65°C; 12 h;
参考文献
Tetrahedron, , vol. 40, # 9 p. 1629 - 1632
反应条件
potassium tert-butylate; dimethyl sulfoxide 2 h; Heating;
参考文献
Pasha; Nagaraja
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2001 , vol. 40, # 12 p. 1172 - 1173
反应条件
perchloric acid in diethyl ether T=25°C; 1 h; Further byproducts given;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 24, p. 820 - 823
反应条件
potassium tert-butylate in dimethyl sulfoxide Ambient temperature;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 34, # 7 p. 636 - 638
反应条件
potassium tert-butylate in tetrahydrofuran T=66°C; 7.5 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Roy, Animesh; Gurudutt, K. N.; Rao, Sanjay
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1995 , vol. 34, # 7 p. 636 - 638
反应条件
potassium tert-butylate in tetrahydrofuran T=66°C; 7.5 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Roy, Animesh; Gurudutt, K. N.; Rao, Sanjay
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1995 , vol. 34, # 7 p. 636 - 638
反应条件
potassium tert-butylate in tetrahydrofuran T=66°C; 7.5 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Roy, Animesh; Gurudutt, K. N.; Rao, Sanjay
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1995 , vol. 34, # 7 p. 636 - 638
