反应条件
1: With n-butyllithium; N,N,N',N'',N''-pentamethyldiethylenetriamine in tetrahydrofuran; hexane
T=-78°C; 3 h;
2: With boric acid trimethyl ester in tetrahydrofuran; hexane
T=20°C; 2 h;
3: With dihydrogen peroxide; acetic acid in tetrahydrofuran; hexane
T=0°C; Further stages.;
参考文献
Zbinden, Katrin Groebke; Banner, David W.; Hilpert, Kurt; Himber, Jacques; Lave, Thierry; Riederer, Markus A.; Stahl, Martin; Tschopp, Thomas B.; Obst-Sander, Ulrike
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 15 p. 5357 - 5369
