4-甲基偶氮苯四氟硼酸盐合成路线 （共 216 条）
反应条件
2,6-di-tert-butyl-4-methylpyridine; gold(I) chloride; palladium dichloride; SIDip*HCl in acetonitrile T=20°C; Sonogashira coupling;
参考文献
Panda, Biswajit; Sarkar, Tarun K.
Chemical Communications, 2010 , vol. 46, # 18 p. 3131 - 3133
反应条件
1: With [Pd2(dibenzylideneacetone)3]*dibenzylideneacetone; sodium acetate in acetonitrile T=30°C; Heck reaction; 0.5 h; 2: With hydrogenchloride in water; acetonitrile T=25°C; 0.5 h;
参考文献
Machado, Angelo H.L.; de Sousa, Marcio A.; Patto, Daniela C.S.; Azevedo, Luiz F.S.; Bombonato, Fernanda I.; Correia, Carlos Roque D.
Tetrahedron Letters, 2009 , vol. 50, # 11 p. 1222 - 1225
反应条件
biscyclopentadienyliron(II) in acetone T=20°C; 3 h; Further byproducts given. Yields of byproduct given;
参考文献
Bragina, I. O.; Kandor, I. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, p. 1411 - 1415
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 7 p. 1594 - 1599
反应条件
potassium acetate; 18-crown-6 ether 1.5 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Beadle, James R.; Korzeniowsky, Stephen H.; Rosenberg, David E.; Garcia-Slanga, Blanche J.; Gokel, George W.
Journal of Organic Chemistry, 1984 , vol. 49, # 9 p. 1594 - 1603
反应条件
biscyclopentadienyliron(II) in acetone T=20°C; 3 h; Further byproducts given. Yields of byproduct given;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 37, p. 1411 - 1415
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 7 p. 1594 - 1599
反应条件
iodine; potassium iodide in dimethyl sulfoxide T=15°C;
参考文献
Citterio, Attilio; Arnold, Anna
Synthetic Communications, 1981 , vol. 11, # 8 p. 639 - 642
反应条件
potassium iodide in water; acetone T=0 - 15°C;
参考文献
Ganushchak, N. I.; Bilaya, E. E.; Obushak, N. D.
J. Gen. Chem. USSR (Engl. Transl.), 1990 , vol. 60, # 2.2 p. 403 - 405,347 - 349
反应条件
β-cyclodextrin; potassium iodide in water T=26°C; variation of pH and reagent; KineticsMechanismProduct distribution;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 991 - 996
反应条件
copper in dimethyl sulfoxide T=20°C; 1 h; other catalyst, other time; Rate constantMechanismProduct distribution;
参考文献
Journal of Chemical Research, Miniprint, , # 4 p. 876 - 890
反应条件
N,N-methylenediacrylamide; Cu(BF4)2*6H2O in water; dimethyl sulfoxide byproducts: 4-MeC6H4CH2CH(SCN)CONHCH2NHCOCHCH2; addn. of 4-MeC6H4N2BF4 (1.1 equiv.) to N,N-methylenediacrylamide (1 equiv.), Cu(BF4)2*6H2O (0.1 equiv.) and NH4SCN (1.1 equiv.) in H2O-DMSO (1:4) for 30 min; evolution of gas at 10-15°C for 45 min;
参考文献
Grishchuk; Baranovskii; Gorbovoi; Ganushchak
Russian Journal of General Chemistry, 2003 , vol. 73, # 6 p. 957 - 960
