4-甲基偶氮苯四氟硼酸盐合成路线 （共 216 条）
反应条件
Cu(BF4)2 in water; acetone addn. of CH3C6H4N2BF4 to 1,4-bis(acryloyloxy)butane, Cu(BF4)2 and NH4SCNin aq. acetone (1:2) for 45-60 min; cooling at -10 - -5°C for 2 h; evolution of N2, treatment of residual with Et2O, extn., washing with water, drying with MgSO4, removal of ether, chromy.;
参考文献
Gorbovoi; Baranovskii; Koval'skii; Grishchuk
Russian Journal of General Chemistry, 2002 , vol. 72, # 8 p. 1230 - 1232
反应条件
DABCO-bis(sulfur dioxide) in acetonitrile T=25°C; 0.333333 h; Inert atmosphere;
参考文献
Zheng, Danqing; An, Yuanyuan; Li, Zhenhua; Wu, Jie
Angewandte Chemie - International Edition, 2014 , vol. 53, # 9 p. 2451 - 2454
Angew. Chem., 2014 , vol. 126, # 9 p. 2483 - 2486,4
反应条件
2,6-di-tert-butyl-4-methylpyridine; gold(I) chloride; palladium dichloride; SIDip*HCl in acetonitrile T=20°C; Sonogashira coupling;
参考文献
Panda, Biswajit; Sarkar, Tarun K.
Chemical Communications, 2010 , vol. 46, # 18 p. 3131 - 3133
反应条件
triethylamine; gold(I) chloride; palladium dichloride in acetonitrile T=20°C; Sonogashira coupling;
参考文献
Panda, Biswajit; Sarkar, Tarun K.
Chemical Communications, 2010 , vol. 46, # 18 p. 3131 - 3133
反应条件
sodium acetate; tris(dibenzylideneacetone)dipalladium (0) in acetonitrile T=25°C; Heck arylation; 2 h; ultrasound; Product distribution; Further Variations:Reaction partnersSolventsTemperaturestime;
参考文献
Burtoloso, Antonio Carlos B.; Garcia, Ariel L. L.; Miranda, Karen C.; Correia, Carlos Roque D.
Synlett, 2006 , # 18 p. 3145 - 3149
反应条件
copper acetylacetonate; copper T=40°C; 0.5 h;
参考文献
Citterio, Attilio; Ferrario, Francesco
Journal of Chemical Research, Miniprint, 1983 , # 12 p. 2656 - 2668
反应条件
potassium acetate; 18-crown-6 ether in chloroform 4 h; Ambient temperature;
参考文献
Luxen, Andre; Christiaens, Leon
Tetrahedron Letters, 1982 , vol. 23, # 38 p. 3905 - 3908
参考文献
Bulletin of the Chemical Society of Japan, , vol. 75, # 4 p. 789 - 800
反应条件
dibenzo-18-crown-6; potassium bromide; copper(ll) bromide; 1,10-phenanthroline; copper(I) bromide in acetonitrile T=20°C; Sandmeyer bromination; 0.333333 h;
参考文献
Beletskaya, Irina P.; Sigeev, Alexander S.; Peregudov, Alexander S.; Petrovskii, Pavel V.
Synthesis, 2007 , # 16 p. 2534 - 2538
反应条件
sodium bromide; copper(ll) bromide in water; acetone T=7 - 20°C; 2.5 h;
参考文献
Russian Journal of General Chemistry, , vol. 66, # 4 p. 623 - 626
