4-甲基偶氮苯四氟硼酸盐合成路线 （共 216 条）
反应条件
palladium diacetate; SIDip*HCl in tetrahydrofuran T=20°C; Mizoroki-Heck coupling; 3 h;
参考文献
Andrus, Merritt B.; Song, Chun; Zhang, Jiuqing
Organic Letters, 2002 , vol. 4, # 12 p. 2079 - 2082
反应条件
SIDip*HCl; palladium diacetate in tetrahydrofuran T=20°C; 1.5 h;
参考文献
Ma, Yudao; Song, Chun; Jiang, Wei; Xue, Guoping; Cannon, John F.; Wang, Xiaomei; Andrus, Merritt B.
Organic Letters, 2003 , vol. 5, # 24 p. 4635 - 4638
反应条件
1: tBuCH2CH2B(H)NiPr2; 4-toluenediazonium tetrafluoroborate With biscyclopentadienyliron(II) in acetonitrile T=20°C; 2.5 h; 2: With methanol in acetonitrile T=0 - 20°C; 1 h; 3: 2,3-dimethylbutane-2,3-diol in diethyl ether; acetonitrile T=20°C; 4 h; SolventReagent/catalyst;
参考文献
UNIVERSITE DE BORDEAUX 1; CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE; PUCHEAULT, Mathieu Jonathan Damien; MARCIASINI, Ludovic Daniel Alain; VAULTIER, Michel
Patent: WO2014/9169 A1, 2014 ;
Location in patent: Page/Page column 53-54 ;
反应条件
potassium acetate in water; acetone T=20°C;
参考文献
Molinaro, Carmela; Mowat, Jeffrey; Gosselin, Francis; O'Shea, Paul D.; Marcoux, Jean-Francois; Angelaud, Remy; Davies, Ian W.
Journal of Organic Chemistry, 2007 , vol. 72, # 5 p. 1856 - 1858
反应条件
2-iodo-propane; copper in dimethyl sulfoxide 3 h; Ambient temperature; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Journal of Chemical Research, Miniprint, , # 4 p. 876 - 890
反应条件
copper in dimethyl sulfoxide T=20°C; 1 h; other catalyst, other time; Rate constantMechanismProduct distribution;
参考文献
Journal of Chemical Research, Miniprint, , # 4 p. 876 - 890
参考文献
Yoneda, Norihiko; Fukuhara, Tsuyoshi; Mizokami, Takao; Suzuki, Akira
Chemistry Letters, 1991 , # 3 p. 459 - 460
反应条件
T=60 - 80°C; 1 h; Yield given. Yields of byproduct given;
参考文献
Yoneda, Norihiko; Fukuhara, Tsuyoshi; Mizokami, Takao; Suzuki, Akira
Chemistry Letters, 1991 , # 3 p. 459 - 460
反应条件
byproducts: N2; equimolar mixture, 60-80°C;
参考文献
Nazaretyan, V. P.; Kamenskaya, O. I.
Zhurnal Organicheskoi Khimii, 1976 , vol. 12, p. 686
Zhurnal Organicheskoi Khimii, 1976 , vol. 12, p. 690
C.A., 1976 , vol. 84, p. 164331
Full Text Show Details
Gmelin Handbook: F: PerFHalOrg.SVol.3, 6.2.3.1, page 48 - 120
反应条件
(3aS,7aS)-1,3-di-o-tolyl-octahydro-benzoimidazole-2-thione; palladium diacetate in tetrahydrofuran T=50°C; Suzuki reaction; 10 h;
参考文献
Mingji, Dai; Liang, Bo; Wang, Cuihua; You, Zejin; Xiang, Jing; Dong, Guangbin; Chen, Jiahua; Yang, Zhen
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1669 - 1673
