4-甲氧苯重氮四氟硼酸盐合成路线 （共 231 条）
反应条件
zinc in carbonic acid dimethyl ester
T=80°C; 0.416667 h; Microwave irradiation;
参考文献
Kundu, Debasish; Ahammed, Sabir; Ranu, Brindaban C.
Green Chemistry, 2012 , vol. 14, # 7 p. 2024 - 2030
反应条件
in tetrahydrofuran
T=20°C; 4 h; Inert atmosphereGreen chemistry; SolventTime;
参考文献
Balaguez, Renata A.; Ricordi, Vanessa Gentil; Freitas, Camilo S.; Perin, Gelson; Schumacher, Ricardo F.; Alves, Diego
Tetrahedron Letters, 2014 , vol. 55, # 5 p. 1057 - 1061
反应条件
in methanol
T=20°C; Substitution; 0.166667 h;
参考文献
Beletskaya; Sigeev; Peregudov; Petrovskii
Russian Journal of Organic Chemistry, 2001 , vol. 37, # 10 p. 1463 - 1475
反应条件
dichloro bis(acetonitrile) palladium(II) in water
T=0 - 40°C; Suzuki-Miyaura Coupling; 4 h;
参考文献
El Bakouri, Ouissam; Fernandez, Marti; Brun, Sandra; Pla-Quintana, Anna; Roglans, Anna
Tetrahedron, 2013 , vol. 69, # 46 p. 9761 - 9765
反应条件
1: sec.-butyllithium With zinc dibromide in tetrahydrofuran; hexane
T=0°C; 0.166667 h; Inert atmosphere;
2: 4-methoxybenzenediazonium tetrafluoroborate With zinc dibromide in tetrahydrofuran
T=-60 - 25°C; Inert atmosphere;
3: in tetrahydrofuran
T=125°C; 2 h; Inert atmosphereMicrowave irradiation; regioselective reaction;
参考文献
Haag, Benjamin A.; Zhang, Zhi-Guang; Li, Jin-Shan; Knochel, Paul
Angewandte Chemie - International Edition, 2010 , vol. 49, # 49 p. 9513 - 9516
反应条件
magnesium
1.) THF, reflux, 2.) THF, 30 deg C, 60 s; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Singh, P. R.; Khanna, R. K.; Jayaraman, B.
Tetrahedron Letters, 1982 , vol. 23, # 51 p. 5475 - 5478
反应条件
tris-(dibenzylideneacetone)dipalladium(0) in acetonitrile
T=20°C; Heck reaction; 0.5 h;
参考文献
Sabino, Adao A.; Machado, Angelo H. L.; Correia, Carlos Roque D.; Eberlin, Marcos N.
Angewandte Chemie - International Edition, 2004 , vol. 43, # 19 p. 2514 - 2518
反应条件
tetra(n-butyl)ammonium hydrogensulfate; palladium diacetate in N,N-dimethyl-formamide
T=25°C; Heck reaction; 5 h;
参考文献
Machado, Angelo H.L.; de Sousa, Marcio A.; Patto, Daniela C.S.; Azevedo, Luiz F.S.; Bombonato, Fernanda I.; Correia, Carlos Roque D.
Tetrahedron Letters, 2009 , vol. 50, # 11 p. 1222 - 1225
反应条件
palladium diacetate; caesium carbonate; potassium iodide in acetonitrile
T=20 - 80°C; Inert atmosphere;
参考文献
Berrino, Roberta; Cacchi, Sandro; Fabrizi, Giancarlo; Goggiamani, Antonella; Stabile, Paolo
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 20 p. 4518 - 4520
反应条件
5 Pd/BaCO3 in methanol
T=25°C; 12 h;
参考文献
Felpin, Francois-Xavier; Fouquet, Eric
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 6 p. 863 - 868
