4-甲氧苯重氮四氟硼酸盐合成路线 （共 231 条）
反应条件
biscyclopentadienyliron(II) in acetone
T=20°C; 3 h; Yields of byproduct given;
参考文献
Bragina, I. O.; Kandor, I. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, p. 1411 - 1415
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 7 p. 1594 - 1599
反应条件
palladium diacetate in acetic acid
T=60 - 100°C; Heck Reaction; 3 h;
参考文献
Lauer, Milena Helmer; Drekener, Roberta Lopes; Correia, Carlos Roque Duarte; Gehlen, Marcelo Henrique
Photochemical and Photobiological Sciences, 2014 , vol. 13, # 6 p. 859 - 866
反应条件
[(t-Bu)2P(OH)]2PdCl2 ; sodium acetate in acetonitrile
Heck Reaction; 1 h; Reflux; Reagent/catalyst;
参考文献
Canto, Karen; Da Silva Ribeiro, Rodrigo; Biajoli, Andre F. P.; Correia, Carlos Roque D.
European Journal of Organic Chemistry, 2013 , # 35 p. 8004 - 8013
反应条件
1.1: palladium diacetate / methanol / 0.08 h / 80 °C / |Microwave irradiation
2.1: sodium hydroxide / water; methanol / 2 h / |Reflux
2.2: 12 h / |Reflux
View Scheme
参考文献
Canto, Karen; Da Silva Ribeiro, Rodrigo; Biajoli, Andre F. P.; Correia, Carlos Roque D.
European Journal of Organic Chemistry, 2013 , # 35 p. 8004 - 8013
反应条件
sodium acetate; tris(dibenzylideneacetone)dipalladium (0) in acetonitrile
T=65°C; Heck arylation; 1 h; Product distribution; Further Variations:ReagentsSolventsTemperaturestime;
参考文献
Canto, Karen; Da Silva Ribeiro, Rodrigo; Biajoli, Andre F. P.; Correia, Carlos Roque D.
European Journal of Organic Chemistry, 2013 , # 35 p. 8004 - 8013
反应条件
1: 4-methoxybenzenediazonium tetrafluoroborate With palladium diacetate in methanol
Suzuki-Miyaura reaction; 0.166667 h; Inert atmosphere;
2: potassium 3,4-(methylenedioxy)phenyltrifluoroborate in methanol
T=20°C; Suzuki-Miyaura reaction; 12 h; Inert atmosphere;
参考文献
Schmidt, Bernd; Hoelter, Frank
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 13 p. 4914 - 4920
反应条件
pyridine; sulfolane
T=20 - 60°C; 8 h; Title compound not separated from byproducts.;
参考文献
Hanson, Peter; Taylor, Alec B.; Walton, Paul H.; Timms, Allan W.
Organic and Biomolecular Chemistry, 2007 , vol. 5, # 4 p. 679 - 698
反应条件
in water; acetone
T=-30 - -25°C; Arylation;
参考文献
Gorbovoi; Zagrichuk; Blinder; Vlasik; Grishchuk
Pharmaceutical Chemistry Journal, 1999 , vol. 33, # 1 p. 22 - 23
反应条件
dibenzo-18-crown-6; Cu(BF4)2; N,N,N',N,-tetramethylethylenediamine; [Cu(CH3CN)4]BF4 in acetonitrile
T=0°C; Sandmeyer Reaction; 1 h;
参考文献
Sigeev, A. S.; Beletskaya, I. P.; Petrovskii, P. V.; Peregudov, A. S.
Russian Journal of Organic Chemistry, 2012 , vol. 48, # 8 p. 1055 - 1058,4
Zhurnal Organicheskoi Khimii, 2012 , vol. 48, # 8 p. 1059 - 1062,4
反应条件
sodium o-benzenedisulfonimide in acetonitrile
T=50°C; 2.5 h;
参考文献
Barbero; Degani; Diulgheroff; Dughera; Fochi
Synthesis, 2001 , # 4 p. 585 - 590
