4-甲氧苯重氮四氟硼酸盐合成路线 (共 231 条)
反应条件
zinc in carbonic acid dimethyl ester
T=80°C; 0.416667 h; Microwave irradiation;
参考文献
Kundu, Debasish; Ahammed, Sabir; Ranu, Brindaban C.
Green Chemistry, 2012 , vol. 14, # 7 p. 2024 - 2030
反应条件
in dimethyl sulfoxide
0.5 h;
参考文献
Petrillo, Giovanni; Novi, Marino; Garbarino, Giacomo; Filiberti, Marcos
Tetrahedron Letters, 1988 , vol. 29, # 33 p. 4185 - 4188
反应条件
in dimethyl sulfoxide
0.833333 h;
参考文献
Petrillo, Giovanni; Novi, Marino; Garbarino, Giacomo; Filiberti, Marcos
Tetrahedron, 1989 , vol. 45, # 23 p. 7411 - 7420
参考文献
Canning, Peter S. J.; Maskill, Howard; McCrudden, Katharine; Sexton, Brian
Bulletin of the Chemical Society of Japan, 2002 , vol. 75, # 4 p. 789 - 800
反应条件
1: 0.0166667 h; Microwave irradiation;
2: With water in diethyl ether
参考文献
Saez, Rebeca; Dolores Otero; Batanero, Belen; Barba, Fructuoso
Journal of Chemical Research, 2008 , # 9 p. 492 - 494
反应条件
1: 54 percent / dimethylformamide / 2 h / 95 °C
2: dimethylformamide / 80 °C
View Scheme
参考文献
Markgraf, J. Hodge; Chang, Raymond; Cort, John R.; Durant Jr., Joseph L.; Finkelstein, Manuel; Gross, Andrew W.; Lavyne, Michael H.; Moore, W. Michael; Petersen, Raymond C.; Ross, Sidney D.
Tetrahedron, 1997 , vol. 53, # 29 p. 10009 - 10018
反应条件
methanol; calcium carbonate
T=25°C; Mirozoki-Heck reaction; Kinetics; Reagent/catalyst; stereoselective reaction;
参考文献
Stern, Therese; Rueckbrod, Sven; Czekelius, Constantin; Donner, Constanze; Brunner, Heiko
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 11-12 p. 1983 - 1992
反应条件
1: 1) NaOAc, CuCl2, 48percent HBF4, 2) AlCl3 / 1) DMF, HOAc, 60 deg C, 2) CH2Cl2, r.t., 3 h
2: 1 M K2CO3 / methanol; H2O / 1.5 h / Heating
View Scheme
参考文献
Wurm; Gurka
Pharmazie, 1997 , vol. 52, # 10 p. 739 - 743
反应条件
sodium acetate in N,N-dimethyl-formamide
1.5 h; Ambient temperature;
参考文献
Takahashi, Ichiro; Muramatsu, Osamu; Fukuhara, Jun; Hosokawa, Yoshinao; Takeyama, Naohiko; et al.
Chemistry Letters, 1994 , # 3 p. 465 - 468
反应条件
palladium on activated charcoal in methanol
T=50°C; Suzuki-Miyaura cross-coupling; 0.333333 h;
参考文献
Taylor, Rachel H.; Felpin, Francois-Xavier
Organic Letters, 2007 , vol. 9, # 15 p. 2911 - 2914