4-甲氧苯重氮四氟硼酸盐合成路线 (共 231 条)
反应条件
sodium acetate in N,N-dimethyl-formamide 1.5 h; Ambient temperature;
参考文献
Takahashi, Ichiro; Muramatsu, Osamu; Fukuhara, Jun; Hosokawa, Yoshinao; Takeyama, Naohiko; et al.
Chemistry Letters, 1994 , # 3 p. 465 - 468
反应条件
2-iodo-propane; copper in dimethyl sulfoxide 3 h; Ambient temperature; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Citterio, Attilio; Vismara, Elena; Bernardi, Rosanna
Journal of Chemical Research, Miniprint, 1983 , # 4 p. 876 - 890
反应条件
phosphate buffer; water in acetonitrile T=25°C; var. pH; Rate constantMechanism;
参考文献
Brown, Kathlynn C.; Doyle, Michael P.
Journal of Organic Chemistry, 1988 , vol. 53, # 14 p. 3255 - 3261
反应条件
copper in dimethyl sulfoxide T=20°C; 1 h; different quinone/isopropyl iodide ratio; other catalyst, other time; other alkyl iodides, benzene diazonium salts; Rate constantMechanismProduct distribution;
参考文献
Citterio, Attilio; Vismara, Elena; Bernardi, Rosanna
Journal of Chemical Research, Miniprint, 1983 , # 4 p. 876 - 890
反应条件
1: iron sulphate heptahydrate / water; dimethyl sulfoxide / Inert atmosphere 2: hydrogenchloride; water; zinc / methanol / 20 °C / Reflux 3: sodium periodate; sodium dichromate; sulfuric acid / water / 20 h / 20 °C 4: thionyl chloride / -10 - 20 °C / Reflux View Scheme
参考文献
Dietz, Friedrich R.; Prechter, Agnes; Groeger, Harald; Heinrich, Markus R.
Tetrahedron Letters, 2011 , vol. 52, # 6 p. 655 - 657
反应条件
KOH adsorbed on neutral alumina in neat (no solvent) 0.25 h; Milling;
参考文献
Mukherjee, Nirmalya; Chatterjee, Tanmay; Ranu, Brindaban C.
Journal of Organic Chemistry, 2013 , vol. 78, # 21 p. 11110 - 11114
反应条件
Yield given. Multistep reaction;
参考文献
Petrillo, Giovanni; Novi, Marino; Garbarino, Giacomo; Filiberti, Marcos
Tetrahedron, 1989 , vol. 45, # 23 p. 7411 - 7420
反应条件
2,4,6-trinitro-phenol in chloroform; water T=0 - 5°C; 0.7 h;
参考文献
Hashida, Yoji; Kubota, Kazuhiro; Sekiguchi, Shizen
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, p. 905 - 910
反应条件
phosphate buffer; 1,2-dichloro-ethane in dichloromethane T=20°C; var. solvents; in the presence of lipophilic organic anions; Rate constant;
参考文献
Iwamoto, Hidetoshi; Kobayashi, Hiroshi; Murer, Pius; Sonoda, Takaaki; Zollinger, Heinrich
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 9 p. 2590 - 2602
反应条件
in water T=25°C; pH 7.0; other catechol and phenol derivatives; rate of oxygen consumption in aerated solutions; Mechanism;
参考文献
Reszka, Krzysztof J.; Chignell, Colin F.
Journal of the American Chemical Society, 1993 , vol. 115, # 17 p. 7752 - 7760