aluminium trichloride other Radiation; a mixt. of GeCl4 and tetraalkylgermane in presence of AlCl3 as catalystin a Pyrex tube is irradiated with a light stream of argon for 30 min at atmospheric pressure (microwave irradiation: 300 W) (Ar); identification by (1)H-NMR, gas chromy.;
参考文献
Laurent, Regis; Laporterie, Andre; Dubac, Jacques; Berlan, Jacques
Organometallics, 1994 , vol. 13, p. 2493 - 2495
in cyclohexane Kinetics; byproducts: CCl3CCl3; Irradiation (UV/VIS); photolysis of Ge-compd. in cyclohexane in the presence of CCl4 at 245 nm at room temp. for 30 min with a 110 W low pressure Hg arc lamp;
sodium hydroxide in water treatment of dibutylgermanium dichloride with 20percent aq. NaOH and then with48percent aq. HBr according to: H.H. Anderson, J. Am. Chem. Soc. 73 (1951) 54 40-5441;
参考文献
Terent'ev; Platonov; Krylova; Egorov; Nikishin
Journal of Organometallic Chemistry, 2009 , vol. 694, # 12 p. 1786 - 1788