6-甲氧基-2-甲基吡啶-3-硼酸合成路线 （共 2 条）
反应条件
1: With n-butyllithium in tetrahydrofuran; hexane T=-70°C; 1 h; Cooling with acetone-dry ice; 2: With tri-isopropoxy-borane in tetrahydrofuran; hexane T=-70 - 20°C; 16.6667 h; Cooling with acetone-dry ice; 3: With acetic acid in tetrahydrofuran; hexane T=20°C; 1 h;
参考文献
Eisai RandD Management Co., Ltd.
Patent: EP1847535 A1, 2007 ;
Location in patent: Page/Page column 123-124 ;
EP 1847535 A1
反应条件
n-butyllithium; acetic acid in tetrahydrofuran; hexane; water; isopropyl alcohol
参考文献
Gilligan, Paul J.
Patent: US2003/125330 A1, 2003 ;
US 20030125330 A1
