1,3-二溴-1,1-二氟丙烷合成路线 （共 9 条）
反应条件
dibenzoyl peroxide T=80°C; 18 h;
参考文献
Seyferth; Simon; Sepelak; Klein
Journal of the American Chemical Society, 1983 , vol. 105, # 14 p. 4634 - 4639
反应条件
dibenzoyl peroxide T=65 - 110°C; P=5171.62 - 10343.2 Torr; 24 h;
参考文献
Honeywell International Inc.
Patent: US2007/161827 A1, 2007 ;
Location in patent: Page/Page column 3 ;
反应条件
hydrogen fluoride; antimony(V) pentachloride T=150°C;
参考文献
Tarrant et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 2783,2787
参考文献
Tarrant et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 2783,2787
反应条件
potassium hydroxide T=115 - 130°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Honeywell International Inc.
Patent: US2007/161827 A1, 2007 ;
Location in patent: Page/Page column 3 ;
参考文献
Blomquist; Longone
Journal of the American Chemical Society, 1957 , vol. 79, p. 4981
反应条件
potassium hydroxide T=115 - 130°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 45, # 11 p. 2273 - 2274
反应条件
potassium hydroxide in ethanol
参考文献
Journal of Organic Chemistry, , vol. 29, p. 1796 - 1800
反应条件
potassium hydroxide; n-butyllithium
1.) 115-130 deg C, 2.) Hexane, THF/Et2O/pentane, -95 deg C, 60 min; Yield given. Multistep reaction;
参考文献
Seyferth, Dietmar; Simon, Robert M.; Sepelak, Dennis J.; Klein, Helmut A.
Journal of Organic Chemistry, 1980 , vol. 45, # 11 p. 2273 - 2274
