1-碘-3,3,3-三氟丙烷合成路线 （共 34 条）
参考文献
Haszeldine
Journal of the Chemical Society, 1951 , p. 2495,2503
反应条件
palladium diacetate; potassium carbonate in N,N-dimethyl-formamide T=200°C; Elimination/Heck domino reaction; 1 h; Inert atmosphereMicrowave irradiation;
参考文献
Organic Letters, , vol. 14, # 4 p. 1146 - 1149
反应条件
copper(l) iodide in tetrahydrofuran T=20°C; Inert atmosphereGlovebox;
参考文献
Janjetovic, Mario; Traeff, Annika M.; Ankner, Tobias; Wettergren, Jenny; Hilmersson, Goeran
Chemical Communications, 2013 , vol. 49, # 18 p. 1826 - 1828
反应条件
silver
T=-123.1 - 76.9°C; activation energy: E(a); Thermodynamic data;
参考文献
Paul, Anumita; Gellman, Andrew J.
Journal of the American Chemical Society, 1995 , vol. 117, # 35 p. 9056 - 9066
参考文献
Haszeldine
Journal of the Chemical Society, 1951 , p. 2495,2503
反应条件
bis-triphenylphosphine-palladium(II) chloride in benzene
T=120°C; P=38000 Torr; 16 h;
参考文献
Shimizu, Rie; Fuchikami, Takamasa
Tetrahedron Letters, 1996 , vol. 37, # 46 p. 8405 - 8408
反应条件
1: 4,4'-dimethyl-2,2'-bipyridine With lithium diisopropyl amide in tetrahydrofuran; hexane
T=-78°C; 3 h;
2: 3-iodo-1,1,1-trifluoropropane in tetrahydrofuran; hexane
T=-78 - 20°C; Further stages.;
参考文献
The Board of Regents, University and Community College System of Nevada on behalf of the; University of Nevada - Las Vegas
Patent: US2006/264414 A1, 2006 ;
Location in patent: Page/Page column 5; 9; 10 ;
反应条件
1: With platinum
T=-178.16°C; P=2E-10 Torr;
2: With hydrogen
T=-178.16 - 226.84°C; P=2E-10 Torr; Activation energy;
参考文献
Ye, Pingping; Gellman, Andrew J.
Journal of the American Chemical Society, 2008 , vol. 130, # 26 p. 8518 - 8526
参考文献
Haszeldine
Journal of the Chemical Society, 1951 , p. 2495,2503
反应条件
mercury(I) fluoride
T=120°C;
参考文献
Haszeldine; Steele
Journal of the Chemical Society, 1953 , p. 1199,1204
