1,1,1,3,3-五氟丙烷合成路线 (共 90 条)
反应条件
hydrogen fluoride; antimony(V) pentachloride T=-20 - 135°C; P=16274.9 - 21446.5 Torr; Autoclave;
参考文献
Wang, Haiyou; Merkel, Daniel C.; Pokrovski, Konstantin A.; Tung, Hsueh Sung; Shankland, Ian
Patent: US2012/271070 A1, 2012 ;
Location in patent: Page/Page column 6 ;
反应条件
hydrogen fluoride; antimony(V) pentachloride T=120°C; P=18751.9 Torr; 21 h;
参考文献
Wilmet, Vincent; Janssens, Francine; Schoebrechts, Jean-Paul
Patent: US2004/19244 A1, 2004 ;
Location in patent: Page 3 ;
反应条件
hydrogen; palladium 10 on activated carbon T=200°C; P=1520.1 Torr;
参考文献
SOLVAY (Societe Anonyme)
Patent: EP1837325 A1, 2007 ;
Location in patent: Page/Page column 2 ;
反应条件
1: With hydrogen fluoride; titanium tetrachloride T=20 - 120°C; P=18617.8 Torr; 1.16667 h; 2: With potassium hydroxide in water
参考文献
Honeywell International Business Machines
Patent: US6844475 B1, 2005 ;
Location in patent: Page column 3 ;
反应条件
hydrogen fluoride; chlorine; fluorinated SbCl5 T=90 - 95°C; P=6965.99 Torr; 500 h;
参考文献
Pokrovski, Konstantin A.; Merkel, Daniel C.; Wang, Haiyou; Tung, Hsueh Sung; Shankland, Ian
Patent: US2012/59200 A1, 2012 ;
Location in patent: Page/Page column 6 ;
参考文献
LaRoche Industries Inc.
Patent: US5616819 A1, 1997 ;
反应条件
hydrogen fluoride; chlorine; antimony(V) pentachloride T=80 - 95°C; P=8517.48 - 10069 Torr;
参考文献
Honeywell International, Inc.
Patent: US2005/90698 A1, 2005 ;
Location in patent: Page/Page column 5 ;
反应条件
hydrogen fluoride; chlorine; antimony(V) pentachloride T=90 - 95°C; P=6965.99 Torr;
参考文献
Merkel, Daniel C.; Wang, Haiyou; Pokrovski, Konstantin A.; Tung, Hsueh Sung; Shankland, Ian
Patent: US2012/184786 A1, 2012 ;
Location in patent: Page/Page column 8 ;
反应条件
hydrogen fluoride; antimony(V) pentachloride; chlorine T=90 - 95°C; P=6965.99 Torr; chemoselective reaction;
参考文献
Pokrovski, Konstantin A.; Merkel, Daniel C.; Wang, Haiyou; Tung, Hsueh Sung
Patent: US2013/261353 A1, 2013 ;
Location in patent: Paragraph 0078; 0079; 0080 ;
反应条件
hydrogen; palladium on activated charcoal T=180°C; P=7600.51 Torr; Industry scale;
参考文献
HONEYWELL INTERNATIONAL INC.
Patent: WO2002/6194 A2, 2002 ;
Location in patent: Page 18 ;